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163937

N,N,N′,N′-四甲基二氨基氯磷酸

technical grade, 90%

别名:

双(二甲胺基)氯酸磷

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关于此项目

线性分子式:
[(CH3)2N]2P(O)Cl
化学文摘社编号:
1605-65-8
分子量:
170.58
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
24850043
EC Number:
216-517-1
Beilstein/REAXYS Number:
471430
MDL number:
MFCD00008302
Assay:
90%
Form:
liquid
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grade

technical grade

Quality Level

100

assay

90%

form

liquid

refractive index

n20/D 1.466 (lit.)

density

1.152 g/mL at 25 °C (lit.)

functional group

phosphoramide

SMILES string

CN(C)P(Cl)(=O)N(C)C

InChI

1S/C4H12ClN2OP/c1-6(2)9(5,8)7(3)4/h1-4H3

InChI key

WYLQARGYFXBZMD-UHFFFAOYSA-N

Application

N,N,N′,N′-Tetramethylphosphorodiamidic chloride was used in the synthesis of (-)-allohedycaryol and C2-symmetric binaphthyl phosphortriamide. It was also used in total synthesis of neohedycaryol.

pictograms

Corrosion
GHS05

signalword

Danger

hcodes

H314

Hazard Classifications

Eye Dam. 1 - Skin Corr. 1B

存储类别

8A - Combustible corrosive hazardous materials

wgk

WGK 3

flash_point_f

235.4 °F - closed cup

flash_point_c

113 °C - closed cup

ppe

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter

法规信息

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历史批次信息供参考:

分析证书(COA)

Lot/Batch Number
00507HK
0507HK
S28113
08013TD

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Adriaan J. Minnaard et al.
The Journal of organic chemistry, 62(8), 2344-2349 (1997-04-18)
The total synthesis of neohedycaryol (4), the C(9)-C(10) double bond regioisomer of the germacrane sesquiterpene hedycaryol, was accomplished in 10 steps from the known dione 6. A Marshall fragmentation of the intermediate mesylate 14 was used to prepare the trans,trans-cyclodeca-1,6-diene
Vladimir N. Zhabinskii et al.
The Journal of organic chemistry, 61(12), 4022-4027 (1996-06-14)
The enantiomer of (+)-allohedycaryol, a germacrane alcohol isolated from giant fennel (Ferula communis L.), has been synthesized, thereby elucidating the relative and absolute stereochemistry of the natural product. The synthesis of (-)-allohedycaryol started from (+)-alpha-cyperone (5) which was available in
A I Meyers et al.
Chirality, 9(5-6), 431-434 (1997-01-01)
By use of an asymmetric Ullmann coupling involving chiral naphthalene oxazolines 1, the title compounds were prepared in good yields and with high diastereoselectivity. Hydrolysis of the binaphthyl oxazolines 2 led to the di-aldehydes 5, which were transformed into the

全球贸易项目编号

货号GTIN
163937-10G04061837655210
163937-50G04061837655227