206563
3-碘三氟甲苯
98%
别名:
3-碘-α,α,α-三氟甲苯
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关于此项目
线性分子式:
IC6H4CF3
化学文摘社编号:
分子量:
272.01
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
206-934-7
MDL number:
产品名称
3-碘三氟甲苯, 98%
InChI key
IGISPMBUGPHLBY-UHFFFAOYSA-N
InChI
1S/C7H4F3I/c8-7(9,10)5-2-1-3-6(11)4-5/h1-4H
SMILES string
FC(F)(F)c1cccc(I)c1
assay
98%
refractive index
n20/D 1.517 (lit.)
bp
82-82.5 °C/25 mmHg (lit.)
density
1.887 g/mL at 25 °C (lit.)
functional group
fluoro
iodo
Quality Level
Application
3-Iodobenzotrifluoride was used in the preparation of zinc 5,10,15,20-tetrakis(3-(trifluoromethyl)phenylethynyl)porphyrin.
General description
Sonogashira coupling reaction between 3-iodobenzotrifluoride and phenylacetylene using a palladium system has been reported.
hcodes
pcodes
Hazard Classifications
Aquatic Chronic 2
存储类别
10 - Combustible liquids
wgk
WGK 3
flash_point_f
158.0 °F - closed cup
flash_point_c
70 °C - closed cup
ppe
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
Rafael Luque et al.
Organic & biomolecular chemistry, 7(8), 1627-1632 (2009-04-04)
An efficient metal-free Sonogashira coupling protocol catalysed by DABCO is reported, where very good conversions and selectivities to the cross-coupling product were obtained under mild reaction conditions. The reported solvent-, phosphane- and metal-free protocol, that uses a cheap base as
Ming-Cheng Kuo et al.
Dalton transactions (Cambridge, England : 2003), (14)(14), 1433-1439 (2007-03-28)
Sonogashira coupling of zinc 5,10,15,20-tetraethynylporphyrin with various phenyl iodides under mild conditions afforded good yields of the corresponding zinc porphyrins. This method is applicable to a variety of aryl iodides including meso-substituted iodoporphyrin to form a conjugated star-shaped multiporphyrin. The
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