CN
检测方案
97%
形式
powder
折射率
n20/D 1.521 (lit.)
bp
158 °C/742 mmHg (lit.)
密度
1.07 g/mL at 25 °C (lit.)
SMILES string
Cc1ncsc1C
InChI
1S/C5H7NS/c1-4-5(2)7-3-6-4/h3H,1-2H3
InChI key
UWSONZCNXUSTKW-UHFFFAOYSA-N
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一般描述
Radical bromination of 4,5-dimethylthiazole using N-bromosuccinimide in the presence of 2,2′-azobisisobutyronitrile yields mono-, tri- and tetrabromo compounds.
应用
4,5-Dimethylthiazole was used in the preparation of 4-(bromomethyl)-5-(dibromomethyl)thiazole.
法规信息
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示例
T1503
货号
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25G
包装规格/数量
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MMYOMAG-74K-13
1000309185
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Mouaffak Al Hariri et al.
The Journal of organic chemistry, 62(2), 405-410 (1997-01-24)
4-(Bromomethyl)-5-(dibromomethyl)thiazole (1) was prepared in good yields by bromination of 4,5-dimethylthiazole with 3.3 equiv of NBS in the presence of AIBN. Treatment of 1 with sodium iodide led to a thiazole o-quinodimethane 2 which was trapped in situ with dienophiles
Selective Bromination of 4, 5-Dimethylthiazole with N-Bromosuccinimide.
Al Hariri M, et al.
European Journal of Organic Chemistry, 1998(4), 593-594 (1998)
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