方案
97%
折射率
n20/D 1.451 (lit.)
沸点
175-178 °C/120 mmHg (lit.)
密度
1.021 g/mL at 25 °C (lit.)
SMILES字符串
CCOC(=O)\C(=C(/C)C)C(=O)OCC
InChI
1S/C10H16O4/c1-5-13-9(11)8(7(3)4)10(12)14-6-2/h5-6H2,1-4H3
InChI key
WEISAZNMMVPNTH-UHFFFAOYSA-N
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一般描述
Reduction of diethyl isopropylidenemalonate with sodium borohydride has been reported.
应用
Diethyl isopropylidenemalonate has been used in the synthesis of retinoids having functional groups at the side-chain terminus.
储存分类代码
10 - Combustible liquids
WGK
WGK 3
闪点(°F)
176.0 °F - closed cup
闪点(°C)
80 °C - closed cup
个人防护装备
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
此项目有
Reduction of alkylidenecyanoacetates with sodium borohydride.
Marshall JA and Carroll RD.
The Journal of Organic Chemistry, 30(8), 2748-2754 (1965)
Y F Shealy et al.
Journal of medicinal chemistry, 31(6), 1124-1130 (1988-06-01)
Retinoids that have two functional groups at the side-chain terminus have been synthesized. The two terminal functional groups are combinations of the carboxyl, carbethoxy, and N-(ethylamino)carbonyl groups. The synthesis route is based on the sodium amide catalyzed condensation of (E,E)-beta-ionylideneacetaldehyde
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