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Merck
CN
  • Analytical comparison and sensory representativity of SAFE, SPME, and Purge and Trap extracts of volatile compounds from pea flour.

Analytical comparison and sensory representativity of SAFE, SPME, and Purge and Trap extracts of volatile compounds from pea flour.

Food chemistry (2012-09-08)
Chloe Murat, Karine Gourrat, Heike Jerosch, Nathalie Cayot
摘要

Pisum sativum is of great economic and nutritional interest due to its protein content. Nevertheless, pea products are underused as a protein source in human food because of their strong beany flavour. Therefore, the objective of this study was to select an efficient and representative method to extract volatile molecules of pea flour. In the first step, three extraction methods were chosen: solid phase micro extraction (SPME); Purge and Trap extraction and solvent assisted flavour evaporation (SAFE). The corresponding extracts were analysed by gas chromatography coupled with mass spectrometry. In the second step, the sensory representativity of the extracts was assessed either by direct gas chromatography-olfactometry for SPME and for Purge and Trap extracts, or by sniffing for the aqueous SAFE extract. It appeared that SAFE extraction was the most suitable method because of its good extraction capacities and its high sensory representativity of the global odour of pea flour.

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Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, StableFlex
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, for use with manual holder
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with autosampler
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, StableFlex, for use with autosampler
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with manual holder or autosampler, fiber L 2 cm
Supelco
SPME 纤维组件聚二甲基硅氧烷 (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 23 ga
Supelco
SPME 纤维组件聚二甲基硅氧烷 (PDMS), df 100 μm(PDMS, needle size 24 ga, for use with manual holder
Supelco
SPME 纤维组件聚二甲基硅氧烷 (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 24 ga
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 75 μm(CAR/PDMS, for use with manual holder, needle size 24 ga
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with autosampler
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 23 ga, StableFlex, for use with autosampler
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, StableFlex, for use with autosampler
Supelco
聚丙烯酸酯 (PA) 固相微萃取萃取头, df 85 μm(PA, for use with autosampler, needle size 23 ga
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with manual holder
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 23 ga, PDMS/DVB StableFlex, for use with autosampler
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 24 ga, for use with autosampler
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with autosampler
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, for use with manual holder, StableFlex fiber
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with manual holder
Supelco
聚丙烯酸酯 (PA) 固相微萃取萃取头, df 85 μm(PA, for use with autosampler, needle size 24 ga
Supelco
SPME 纤维组件聚二甲基硅氧烷 (PDMS), df 100 μm(PDMS, for use with manual holder, needle size 23 ga
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with autosampler
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, for use with autosampler, needle size 23 ga
Supelco
固相微萃取 StableFlex 萃取头组合套件, for use with manual holder
Supelco
Carbowax-聚乙二醇 (PEG) 固相微萃取萃取头, needle size 23 ga, df 60 μm(PEG, for use with autosampler
Supelco
固相微萃取 StableFlex 萃取头组合套件, needle size 23 ga, for use with autosampler
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with manual holder
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), for use with autosampler, needle size 23 ga, metal alloy fiber, fiber L 2 cm
Supelco
聚丙烯酸酯 (PA) 固相微萃取萃取头, df 85 μm(PA, for use with manual holder, needle size 24 ga
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), fused silica fiber, df 65 μm(PDMS/DVB, for use with manual holder, needle size 23 ga