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194972

tert-Butylhydrazine hydrochloride

Name: <I>tert</I>-Butylhydrazine hydrochloride
Brand: ALDRICH

98%

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About This Item

Linear Formula:

(CH₃)₃CNHNH₂ · HCl

CAS Number:

7400-27-3

Molecular Weight:

124.61

UNSPSC Code:

12352100

NACRES:

NA.22

PubChem Substance ID:

24851664

EC Number:

231-001-6

Beilstein/REAXYS Number:

3651224

MDL number:

MFCD00012947

Assay:

98%

Form:

solid

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Properties

Quality Level

100

assay

98%

form

solid

mp

191-194 °C (lit.)

functional group

amine, hydrazine

SMILES string

Cl.CC(C)(C)NN

InChI

1S/C4H12N2.ClH/c1-4(2,3)6-5;/h6H,5H2,1-3H3;1H

InChI key

DDPWVABNMBRBFI-UHFFFAOYSA-N

Description

Application

tert-Butylhydrazine hydrochloride was used in the synthesis of:

diphosphinohydrazines
5-amino-1-tert-butyl-3-(p-chlorophenyl)-4-cyanopyrazole
1,3,4,5-tetrasubstituted pyrazole derivatives

Storage Class

11 - Combustible Solids

wgk

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

Regulatory Information

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One-pot synthesis of tetrasubstituted pyrazoles-Proof of regiochemistry.

Hanefeld U, et al.

Journal of the Chemical Society. Perkin Transactions 1, 13, 1545-1552 (1996)

Regioselective synthesis of 1, 3, 4, 5-tetrasubstituted pyrazoles from Baylis-Hillman adducts.

Lee KY, et al.

Tetrahedron Letters, 44(35), 6737-6740 (2003)

The intramolecular rearrangement of phosphinohydrazides [R'2P-NR-NR-M] → [RN═PR'2-NR-M]: general rules and exceptions. transformations of bulky phosphinohydrazines (R-NH-N(PPh2)2, R = tBu, Ph2P).

Alexander N Kornev et al.

Inorganic chemistry, 51(2), 874-881 (2012-01-03)

Reactions of diphosphinohydrazines R-NH-N(PPh(2))(2) (R = tBu (1), Ph(2)P (3)) with some metalation reagents (Co[N(SiMe(3))(2)](2), LiN(SiMe(3))(2), La[N(SiMe(3))(2)](3), nBuLi, MeLi) were performed. Compound 1 was synthesized by the reaction of Ph(2)PCl with tert-butylhydrazine hydrochloride in 83% yield. This compound reveals temperature-dependent

Global Trade Item Number

SKU	GTIN
194972-500G	04061832106427
194972-5G	04061832088853
194972-100G	04061838761392