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302325

2-Chloroethanesulfonyl chloride

Name: 2-Chloroethanesulfonyl chloride
Brand: ALDRICH

96%

Synonym(s):

2-Chloro-1-ethanesulfonyl chloride

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About This Item

Linear Formula:

ClCH₂CH₂SO₂Cl

CAS Number:

1622-32-8

Molecular Weight:

163.02

UNSPSC Code:

12352100

NACRES:

NA.22

PubChem Substance ID:

24858246

EC Number:

216-594-1

Beilstein/REAXYS Number:

1751202

MDL number:

MFCD00007461

Assay:

96%

Form:

liquid

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Properties

vapor pressure

15 mmHg ( 84 °C)

Quality Level

200

assay

96%

form

liquid

refractive index

n20/D 1.493 (lit.)

bp

84-86 °C/15 mmHg (lit.)

density

1.56 g/mL at 25 °C (lit.)

functional group

chloro

SMILES string

ClCCS(Cl)(=O)=O

InChI

1S/C2H4Cl2O2S/c3-1-2-7(4,5)6/h1-2H2

InChI key

VHCSBTPOPKFYIU-UHFFFAOYSA-N

Description

Application

2-Chloroethanesulfonyl chloride was used in one-pot sulfonylation/intramolecular thia-Michael protocol for the synthesis of 1,5,2-dithiazepine 1,1-dioxides. It was also used in synthesis of vinylsulfonamides with a furan, carbocyclic, semicyclic or acyclic 1,3-diene moiety.

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pictograms

GHS06,GHS05

signalword

Danger

hcodes

H301,H314,H330,H335

pcodes

P260 - P271 - P280 - P303 + P361 + P353 - P304 + P340 + P310 - P305 + P351 + P338

Hazard Classifications

Acute Tox. 1 Inhalation - Acute Tox. 3 Oral - Eye Dam. 1 - Skin Corr. 1B - STOT SE 3

target_organs

Respiratory system

Storage Class

6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials

wgk

WGK 3

flash_point_f

>230.0 °F

flash_point_c

> 110 °C

ppe

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter

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Synthesis of a Library of 1,5,2-Dithiazepine 1,1-Dioxides. Part 1: A One-Pot Sulfonylation/Thia-Michael Protocol.

Qin Zang et al.

Heterocycles, 86(2), doi:10-doi:10 (2014-01-05)

A novel one-pot sulfonylation/intramolecular thia-Michael protocol is reported for the synthesis of 1,5,2-dithiazepine 1,1-dioxides. Sulfonylation between cysteine ethyl ester/cysteamine and 2-chloroethanesulfonyl chloride, followed by

Thermal and high pressure intramolecular Diels-Alder reaction of vinylsulfonamides.

Victor O Rogachev et al.

Nature protocols, 1(6), 3076-3087 (2007-04-05)

Vinylsulfonamides with a furan, carbocyclic, semicyclic or acyclic 1,3-diene moiety are synthetized via a domino elimination-amidation reaction of 2-chloroethanesulfonyl chloride. Intramolecular Diels-Alder reaction of these vinylsulfonamides with thermal (toluene, 110 degrees C) or high pressure (dichloromethane, 13 kbar) activation provides

Global Trade Item Number

SKU	GTIN
302325-5G	04061837246937
302325-25G	04061837246920