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Merck
CN

M9653

Methoxyacetyl chloride

97%

Synonym(s):

2-methoxyacetyl chloride, Methoxyacetic acid chloride

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About This Item

Linear Formula:
CH3OCH2COCl
CAS Number:
38870-89-2
Molecular Weight:
108.52
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
24897347
EC Number:
254-169-2
Beilstein/REAXYS Number:
1740244
MDL number:
MFCD00000728
Assay:
97%
Form:
liquid

Key Documents

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InChI key

JJKWHOSQTYYFAE-UHFFFAOYSA-N

InChI

1S/C3H5ClO2/c1-6-2-3(4)5/h2H2,1H3

SMILES string

COCC(Cl)=O

assay

97%

form

liquid

refractive index

n20/D 1.419 (lit.)

bp

112-113 °C (lit.)

density

1.187 g/mL at 25 °C (lit.)

storage temp.

2-8°C

Quality Level

100

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Application

Methoxyacetyl chloride can be used for methoxyacetylation of:
  • Bilocularin A to synthesize 8-Methoxyacetoxybilocularin A.
  • Substituted and unsubstituted benzamides to synthesize N-(2-methoxyacetyl)-benzamides.

It can also be used for the synthesis of β-lactams by reacting with imines. and in the post-synthetic modification of the metal-organic framework (MOF), MIL-101, to synthesize a catalyst for cycloaddition reaction of CO2 with propylene oxide.

signalword

Danger

Hazard Classifications

Acute Tox. 3 Inhalation - Eye Dam. 1 - Flam. Liq. 3 - Skin Corr. 1B - STOT SE 3

target_organs

Respiratory system

Storage Class

3 - Flammable liquids

wgk

WGK 3

flash_point_f

82.4 °F

flash_point_c

28 °C

ppe

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter

Regulatory Information

危险化学品
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Certificates of Analysis (COA)

Lot/Batch Number
S10176
18006AN
03231CW
06107PG
03422MY

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Functionalized MIL-101 with imidazolium-based ionic liquids for the cycloaddition of CO2 and epoxides under mild condition.
Liu D, et al.
Applied Surface Science, 428(45), 218-225 (2018)
An investigation towards the diastereoselective synthesis of 3-acetoxy/methoxy/phthalimido-β-lactams using chiral imines.
Bhalla A, et al.
Tetrahedron Asymmetry, 28(2), 307-316 (2017)
Bioactive dihydro-?-agarofuran sesquiterpenoids from the Australian rainforest plant Maytenus bilocularis.
Wibowo M, et al.
Journal of Natural Products, 79(5), 1445-1453 (2016)
Radu A Gropeanu et al.
PloS one, 7(9), e43657-e43657 (2012-09-13)
Three different variants of photoactivatable caged paclitaxel (PTX) have been synthesized and their bioactivity was characterized in in vitro assays and in living cells. The caged PTXs contain the photoremovable chromophore 4,5-dimethoxy-2-nitrobenzyloxycarbonyl (Nvoc) attached to position C7, C2' and to
A telescopic one-pot synthesis of ?-lactam rings using amines as a convenient source of imines.
Rajamaki SHM, et al.
Royal Society of Chemistry Advances, 6(45), 38553-38557 (2016)
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