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Merck
CN

34010

2-NP-AHD-13C3

VETRANAL®, analytical standard

Synonym(s):

1-(2-Nitrobenzylidenamino)-2,4-imidazolidinedione-[2,4,5-13C]

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About This Item

Empirical Formula (Hill Notation):
13C3C7H8N4O4
CAS Number:
1007476-86-9
Molecular Weight:
251.17
NACRES:
NA.24
PubChem Substance ID:
329754755
UNSPSC Code:
41116107
MDL number:
MFCD07366661

Key Documents

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Product Name

2-NP-AHD-13C3, VETRANAL®, analytical standard

InChI

1S/C10H8N4O4/c15-9-6-13(10(16)12-9)11-5-7-3-1-2-4-8(7)14(17)18/h1-5H,6H2,(H,12,15,16)/b11-5+/i6+1,9+1,10+1

SMILES string

[O-][N+](=O)c1ccccc1\C=N\N2[13CH2][13C](=O)N[13C]2=O

InChI key

FULJCJZKZXOFQZ-OTQLJULOSA-N

grade

analytical standard

product line

VETRANAL®

shelf life

limited shelf life, expiry date on the label

technique(s)

HPLC: suitable
gas chromatography (GC): suitable

application(s)

forensics and toxicology
pharmaceutical (small molecule)

format

neat

mass shift

M+3

Quality Level

100

Related Categories

Application

2-NP-AHD-13C3 may be used as a standard in the determination of nitrofuran metabolites and chloramphenicol in shrimp, using single extraction method and liquid chromatographic/mass spectrometric method (LC/MS-MS).
2-NP-AHD-13C3 may be used as an internal standard to quantify the presence of 1-(2-nitrobenzylidenamino)-2,4-imidazolidine-dione (2-NP-AHD) in shrimp samples using liquid chromatography coupled to tandem mass spectrometry (LC-MS/MS).
Refer to the product′s Certificate of Analysis for more information on a suitable instrument technique. Contact Technical Service for further support.

Legal Information

VETRANAL is a registered trademark of Merck KGaA, Darmstadt, Germany

Storage Class

10 - Combustible liquids

wgk

WGK 3

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Certificates of Analysis (COA)

Lot/Batch Number
BCCN3251
BCCL1069
BCCF7828
BCCD5178
BCCD2332

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Simultaneous determination of nitrofuran metabolites and chloramphenicol in shrimp with a single extraction and LC-MS/MS analysis.
El-Demerdash A, et al.
Journal of AOAC (Association of Official Analytical Chemists) International, 98(3), 595-601 (2015)
Aref El-Demerdash et al.
Journal of AOAC International, 98(3), 595-601 (2015-05-31)
A method has been developed to quantify the nitrofuran metabolites 3-amino-5-morphorinomethyl-1,3-oxazolidinone, 3-amino-oxazolidinone, 1-aminohydantoin, and semicarbazide, as well as chloramphenicol in shrimp with a single extraction procedure followed by LC-MS/MS analysis. Dynamic selected reaction monitoring with positive and negative ionization mode

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