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Merck
CN

46384

Florisil® Inorganic Adsorbent

30-60 mesh

Synonym(s):

Florisil®, Activated magnesium silicate, Magnesium silicate

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About This Item

Empirical Formula (Hill Notation):
MgO3Si
CAS Number:
1343-88-0
Molecular Weight:
100.39
NACRES:
SB.52
PubChem Substance ID:
329757158
UNSPSC Code:
23201100
EC Number:
215-681-1
MDL number:
MFCD00078249

Key Documents

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Product Name

Florisil® Adsorbent for Chromatography, 30-60 mesh

InChI key

FKHIFSZMMVMEQY-UHFFFAOYSA-N

InChI

1S/Mg.O3Si/c;1-4(2)3/q+2;-2

SMILES string

[Mg++].[O-][Si]([O-])=O

grade

standard

form

granular

technique(s)

LPLC: suitable

matrix

Magnesium silicate hydrate

matrix active group

magnesium silicate hydrate

particle size

250-595 μm
30-60 mesh

pore size

60 Å mean pore size

separation technique

hydrophilic interaction (HILIC)

Quality Level

100

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Application

Florisil was used:
  • as column packing material in column chromatography
  • as an adsorbent in Gas chromatography with electron capture detector (GC/ECD), capillary column chromatography, adsorption column chromatography
  • in clean-up procedures in gas chromatography-tandem mass spectrometry and GC-FID

General description

Florisil, adsorbent for the separation of lipids, is a commercially-prepared magnesia silica gel. It has a coarse mesh size which helps in rapid flow rate. Florisil is effective in promoting [1,3]-sigmatropic shift of myceophenolic acid related allyl phenyl ethers. Florisil cartridges are used in atmospheric sampling to assess possible interference from air contaminants.

Legal Information

Florisil is a registered trademark of U.S. Silica Company

Storage Class

13 - Non Combustible Solids

wgk

nwg

flash_point_f

Not applicable

flash_point_c

Not applicable

ppe

Eyeshields, Gloves, type N95 (US)

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Certificates of Analysis (COA)

Lot/Batch Number
BCCN2228
BCCM4242
BCCL4531
BCCL5616
BCCK7772

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An improved gas chromatographic method for the determination of perfluorocarbon tracers in the atmosphere
Lagomarsino, Raymond J.
Journal of Chromatography A, 34, 405-412 (1996)
Andrew C Singer et al.
Environmental toxicology and chemistry, 22(9), 1998-2004 (2003-09-10)
This study investigated the interactive effects of bioaugmentation, biostimulation, and the rhizosphere during remediation of Aroclor 1242-contaminated soil. Treatments were repeatedly augmented with polychlorinated bipheny (PCB)-degrading bacteria, inducers (carvone and salicylic acid), surfactant (sorbitan trioleate), minimal salts medium in a
R C Prados-Rosales et al.
Journal of chromatography. A, 993(1-2), 121-129 (2003-05-09)
A rapid analytical method for determination of organochlorine pesticide residues in sunflower seeds based on focused microwave-assisted Soxhlet extraction has been developed. The main factors affecting the extraction efficiency--namely microwave power, irradiation time, volume of extractant and number of cycles--were
P A de Paula Pereira et al.
Talanta, 49(2), 245-252 (2008-10-31)
A new sampling protocol was developed to determine methanol and ethanol in the gas phase, at low concentration levels, in urban atmospheres. The procedure involves collection of air samples (20.0-30.0 l) with three florisil cartridges connected in series, at a
The Florisil? catalyzed [1, 3]-sigmatropic shift of allyl phenyl ethers-An entryway into novel mycophenolic acid analogues.
Talamas, Francisco X., et al.
Tetrahedron Letters, 38, 4725-4728 (1997)
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