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90479

Glyphosate-2-13C,15N

PESTANAL®, analytical standard

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About This Item

Linear Formula:
HO2C13CH215NHCH2PO3H2
CAS Number:
285978-24-7
Molecular Weight:
171.06
NACRES:
NA.24
PubChem Substance ID:
329769915
UNSPSC Code:
77101502
MDL number:
MFCD01075407
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grade

analytical standard

Quality Level

200

product line

PESTANAL®

assay

≥99% (HPLC)

shelf life

limited shelf life, expiry date on the label

impurities

≤0.5% water

mp

230 °C (dec.) (lit.)

application(s)

agriculture
environmental

format

neat

mass shift

M+2

SMILES string

OC(=O)[13CH2][15NH]CP(O)(O)=O

InChI

1S/C3H8NO5P/c5-3(6)1-4-2-10(7,8)9/h4H,1-2H2,(H,5,6)(H2,7,8,9)/i1+1,4+1

InChI key

XDDAORKBJWWYJS-VFZPYAPFSA-N

General description

Glyphosate is one of the most used herbicides, especially in agriculture applications such as weed and vegetation control.

Application

Glyphosate-2-13C,15N may be used as a reference standard for the determination of glyphosate-2-13C,15N in saline natural water samples by high-performance liquid chromatography coupled to tandem mass spectrometry (HPLC-MS/MS). It may also be used as an internal standard for the analysis of glyphosate, aminomethylphosphonic acid and glufosinate in water samples by online solid-phase extraction (SPE) followed by HPLC/MS.

Analysis Note

13C enrichment ≥99 atom% based upon labeld precursor
15N enrichment ≥98 atom% based upon labeld precursor

Legal Information

PESTANAL is a registered trademark of Merck KGaA, Darmstadt, Germany

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Danger

Hazard Classifications

Acute Tox. 4 Dermal - Aquatic Chronic 2 - Eye Dam. 1

Storage Class

11 - Combustible Solids

wgk

WGK 2

flash_point_f

Not applicable

flash_point_c

Not applicable

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Certificates of Analysis (COA)

Lot/Batch Number
BCCL9604
BCCJ4513
BCCG3972
BCCB5290
BCBZ3625

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Articles

LC/MS/MS Method for Determination of Glyphosate, AMPA, and Glufosinate in Cereals

Glyphosate and related compounds are measured in oatmeal and infant cereal using ion-exchange polymer-based particles for HPLC and SPE. Low level detection was obtained.

Simplified LC-MS/MS for Herbicides in Cereals

Glyphosate analysis: LC-MS/MS method with Supel™ Carbon LC U/HPLC column for stability and retention.

LC/MS/MS法测定谷物中的草甘膦、AMPA和草铵膦

使用 HPLC 和 SPE 的离子交换聚合物基颗粒测定燕麦片和婴儿谷物中的草甘膦及相关化合物。获得低水平的检测结果。

Methods of analysis by the US geological survey organic geochemistry research group-determination of glyphosate, aminomethylphosphonic acid, and glufosinate in water using online solid-phase extraction and high-performance liquid chromatography/mass spectrometry
Lee EA, et al.
Journal of Chromatography and Separation Techniques, 7(338), 2-2 (2002)
Optimization of an Enrichment and LC-MS/MS Method for the Analysis of Glyphosate and Aminomethylphosphonic Acid (AMPA) in Saline Natural Water Samples without Derivatization
Pupke D, et al.
Journal of Chromatography and Separation Techniques, 7(338), 2-2 (2016)
Lene Nørby Nielsen et al.
Environmental pollution (Barking, Essex : 1987), 233, 364-376 (2017-11-03)
Recently, concerns have been raised that residues of glyphosate-based herbicides may interfere with the homeostasis of the intestinal bacterial community and thereby affect the health of humans or animals. The biochemical pathway for aromatic amino acid synthesis (Shikimate pathway), which

Global Trade Item Number

SKUGTIN
90479-5MG04061833246962