11041-U
Carboxen® Adsorbent
matrix Carboxen 1006, 2 μm, bottle of 20 g
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About This Item
UNSPSC Code:
23201100
EC Number:
231-153-3
NACRES:
SB.52
product line
Carboxen®
form
powder
packaging
bottle of 20 g
technique(s)
LPLC: suitable
surface area
~715 m2/g
matrix
Carboxen 1006
matrix active group
carbon
particle size
2 μm
pore size
~0.23 cm3/g macroporosity, ~0.26 cm3/g mesoporosity, ~0.29 cm3/g microporosity, ~7-10 Å pore diameter
density
~0.26 g/mL (free fall density)
separation technique
reversed phase
Quality Level
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General description
Carboxen® adsorbent is ideally used for solid-phase microextraction (SPME). It is highly efficient in extraction of small polar molecules from aqueous solution.
Carboxens are a highly engineered synthetic carbon adsorbent engineered from polymeric precursors. These particles will not plastically deform like resins or generate fines like activated carbon. These materials are shipped and stored dried. These derivatized resins bring value to a wide range of purification applications for removing both small and large molecule impurities. They find use in both gas and liquid phase purifications. Some examples include removal of homogenous catalysts from active pharmaceutical ingredients (API)s, high-risk impurities in biochemical purifications such as host cell proteins from mAbs, removal of toxic heavy metals, purification of chlorinated molecules, and removal of extractables and leachables. Tapered pores result in increased thermodynamic and kinetic properties for both adsorption and desorption. The Carboxens vary in the relative percentage of pore structures (micro, meso, and macro), surface area, and surface pH.
Application
Carboxen® 1006 was used as an extraction device for the determination of ochratoxins A and B in nuts and grain samples using an automated in-tube solid-phase microextraction (SPME) coupled with liquid chromatography-mass spectrometry (LC-MS).
Features and Benefits
Features and Benefits:
- Spherical
- Hard (ball pan hardness >98%)
- Stable up to 400°C
- High purity
- Easy to pack
- Stable over entire pH range
- Do not create backpressure
- High osmotic shock stability
- Tapered pore sizing (from macro- to meso- to micro-)
Other Notes
For more information, please visit: specialty Carbon Adsorbents
Legal Information
Carboxen is a registered trademark of Merck KGaA, Darmstadt, Germany
Storage Class
11 - Combustible Solids
wgk
nwg
flash_point_f
Not applicable
flash_point_c
Not applicable
Regulatory Information
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Applications of Solid Phase Microextraction.
Pawliszyn J.
Science, 64-65 (1999)
Keita Saito et al.
Journal of chromatography. A, 1220, 1-6 (2011-12-20)
A simple and sensitive method for the determination of ochratoxins A and B in nuts and grain samples was developed using an automated in-tube solid-phase microextraction (SPME) coupled with liquid chromatography-mass spectrometry (LC-MS). Ochratoxins were separated within 5 min by
B D Page et al.
Journal of chromatography. A, 873(1), 79-94 (2000-04-11)
The headspace solid-phase microextraction (HS-SPME) efficiencies from vegetable oil of the recently available Carboxen-poly(dimethylsiloxane) (PDMS) and divinylbenzene-Carboxen-PDMS fibres were found to be much greater than those of the PDMS fibre for a number of volatile contaminants. Using these Carboxen-based fibres
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