质量水平
方案
98%
表单
chunks
沸点
241 °C (lit.)
mp
43-47 °C (lit.)
密度
1.112 g/mL at 25 °C (lit.)
SMILES字符串
COc1cccc(OC)c1OC
InChI
1S/C9H12O3/c1-10-7-5-4-6-8(11-2)9(7)12-3/h4-6H,1-3H3
InChI key
CRUILBNAQILVHZ-UHFFFAOYSA-N
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一般描述
1,2,3-三甲氧基苯与2,4-二氨基-5-(羟甲基)嘧啶发生缩合反应，得到2,4-二氨基-5-(2,3,4-三甲氧基苄基)嘧啶。
应用
1,2,3-三甲氧基苯用于研究溶剂对光致电子转移反应的影响。
储存分类代码
11 - Combustible Solids
WGK
WGK 3
闪点(°F)
235.4 °F - closed cup
闪点(°C)
113 °C - closed cup
个人防护装备
Eyeshields, Gloves, type N95 (US)
Romelo Gibe et al.
Chemical communications (Cambridge, England), (14)(14), 1550-1551 (2002-08-23)
Nicholas reactions of the p-phenyl linked bis(propargyl acetate) complex (3a) with electron rich arenes give cyclophanetetrayne complexes (5). The use of bis(propargyl ether) complex (8) with (3a) allows formation of a mixed cyclophanetetrayne complex (9), and in addition gives retro-Nicholas/intramolecular
Zhangjie Shi et al.
Journal of the American Chemical Society, 126(19), 5964-5965 (2004-05-13)
A gold-catalyzed cyclialkylation of electron-rich arenes with tethered epoxides afforded 3-chromanols stereospecifically.
A Stuart et al.
Journal of medicinal chemistry, 26(5), 667-673 (1983-05-01)
A new route to 2,4-diamino-5-(4-hydroxybenzyl)pyrimidines has been developed that involves the condensation of 2,4-diamino-5-(hydroxymethyl)pyrimidine with phenols in acidic medium. The use of phenol and its 2,6-dialkyl derivatives produces 5-(4-hydroxybenzyl)pyrimidines exclusively. However, 2,6-dimethoxyphenol produces a mixture of 5-(3-hydroxy-2,4-dimethoxybenzyl)- and 5-(4-hydroxy-3,5-dimethoxybenzyl)pyrimidines. The
Liming Zhang et al.
Magnetic resonance in chemistry : MRC, 45(1), 37-45 (2006-11-03)
A new analytical method based on the 2D HSQC NMR sequence is presented, which can be applied for quantitative structural determination of complicated polymers. The influence of T1 and T2 relaxations, off-resonance effects, coupling constants and homonuclear couplings are discussed.
Ramjee Kandel et al.
Dalton transactions (Cambridge, England : 2003), 48(33), 12512-12521 (2019-08-01)
Phosphaamidine metal complexes Rh2Cl2[Ph2PC(Ph)[double bond, length as m-dash]NPh]2μ-CO (1), RuCl2[Ph2PC(Ph)[double bond, length as m-dash]N(Ph)]2 (2), [Rh{iPr2PC(Ph)[double bond, length as m-dash]NiPr}(COD)]BF4 (3), and RuCl2[iPr2PC(Ph)[double bond, length as m-dash]NiPr](DMSO)2 (4) are prepared by combining phosphaamidines Ph2P-C(Ph)[double bond, length as m-dash]NPh and iPr2P-C(Ph)[double
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