Merck
CN

186708

Sigma-Aldrich

(S)-(+)-2-氨基-3-甲基-1-丁醇

96%

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别名:
L-缬氨醇
线性分子式:
(CH3)2CHCH(NH2)CH2OH
CAS号:
分子量:
103.16
Beilstein:
1719137
EC 号:
MDL编号:
PubChem化学物质编号:
NACRES:
NA.22

质量水平

检测方案

96%

旋光性

[α]25/D +10°, c = 10 in H2O

光学纯度

ee: 95% (GLC)

折射率

n20/D 1.4548 (lit.)

bp

81 °C/8 mmHg (lit.)

mp

30-32 °C (lit.)

密度

0.926 g/mL at 25 °C (lit.)

储存温度

2-8°C

SMILES string

CC(C)[C@H](N)CO

InChI

1S/C5H13NO/c1-4(2)5(6)3-7/h4-5,7H,3,6H2,1-2H3/t5-/m1/s1

InChI key

NWYYWIJOWOLJNR-RXMQYKEDSA-N

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Sigma-Aldrich

293520

羰苄氧基-L-缬氨酸

refractive index

n20/D 1.4548 (lit.)

refractive index

n20/D 1.425 (lit.)

refractive index

-

refractive index

-

bp

81 °C/8 mmHg (lit.)

bp

84-86 °C/15 mmHg (lit.)

bp

-

bp

-

mp

30-32 °C (lit.)

mp

-

mp

62-64 °C (lit.)

mp

35-36 °C (lit.)

density

0.926 g/mL at 25 °C (lit.)

density

1.106 g/mL at 25 °C (lit.)

density

-

density

-

storage temp.

2-8°C

storage temp.

-

storage temp.

-

storage temp.

-

应用

(S)-(+)-2-氨基-3-甲基-1-丁醇可用于制备:
  • 亚胺和噁唑啉(分别通过与醛和腈反应生成)。
  • 含环三磷腈基元的手性噁唑啉衍生多齿配体。

储存分类代码

10 - Combustible liquids

WGK

WGK 3

闪点(°F)

172.4 °F - closed cup

闪点(°C)

78 °C - closed cup

个人防护装备

dust mask type N95 (US), Eyeshields, Gloves

法规信息

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Journal of the Chemical Society. Perkin Transactions 1, 192-192 (1989)
Tetrahedron Letters, 34, 2015-2015 (1993)
Dheeraj Kumar et al.
Dalton transactions (Cambridge, England : 2003), 43(37), 13899-13912 (2014-08-12)
Chiral oxazoline based bi and hexadentate ligands built on cyclophosphazene cores have been synthesized and characterized. (NPPh2)2[NP(m-OC6H4C(O)OCH3)2] (1) was prepared by the reaction of gem-(NPPh2)2(NPCl2) with methyl-3-hydroxy benzoate in the presence of Cs2CO3. Compound 1 was converted to the dicarboxylic
Carla Fernandes et al.
Chirality, 29(8), 430-442 (2017-06-14)
Six chiral derivatives of xanthones (CDXs) were covalently bonded to silica, yielding the corresponding xanthonic chiral stationary phases (XCSPs). The new XCSPs were packed into stainless-steel columns with 150 x 4.6 mm i.d. Moreover, the greening of the chromatographic analysis
Enantioselective palladium catalysed allylic substitution with thienyl oxazoline ligands
Frost CG and Williams JMJ
Tetrahedron Letters, 34(12), 2015-2018 (1993)

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