198005
2-氯-1-甲基吡啶碘化物
97%
别名:
Mukaiyama试剂
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关于此项目
经验公式（希尔记法）:
C6H7ClIN
化学文摘社编号:
分子量:
255.48
Beilstein:
3572320
EC 号:
MDL编号:
UNSPSC代码:
12352100
PubChem化学物质编号:
NACRES:
NA.22
质量水平
方案
97%
mp
200 °C (dec.) (lit.)
官能团
chloro
SMILES字符串
[I-].C[n+]1ccccc1Cl
InChI
1S/C6H7ClN.HI/c1-8-5-3-2-4-6(8)7;/h2-5H,1H3;1H/q+1;/p-1
InChI key
ABFPKTQEQNICFT-UHFFFAOYSA-M
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一般描述
2-氯-1-甲基吡啶碘化物（Mukaiyama试剂）是有机合成中的常用试剂，用于活化醇的羟基和羧酸。它可用于以相应的羧酸合成酯、内酯、酰胺、内酰胺和烯酮的衍生物。由于其毒性低、反应条件简单、价格比EDC便宜，它还可用作肽合成中的高效偶联剂。
应用
2-氯-1-甲基吡啶碘化物（CMPI）可用作：
- 脱水剂，用于将各种醛肟转化为腈，醇转化为硫氰酸烷基酯。
- 交联剂，用于制备用于生物医学应用的可生物降解交联透明质酸膜和明胶膜。
- 缩合剂，用于以β氨基酸合成各种β内酰胺。
储存分类代码
11 - Combustible Solids
WGK
WGK 3
闪点(°F)
Not applicable
闪点(°C)
Not applicable
个人防护装备
dust mask type N95 (US), Eyeshields, Gloves
历史批次信息供参考:
分析证书(COA)
Lot/Batch Number
A novel cell support membrane for skin tissue engineering: Gelatin film cross-linked with 2-chloro-1-methylpyridinium iodide
Yeh Ming-kung, et al.
Polymer, 52(4), 996-1003 (2011)
Ming-Kung Yeh et al.
Journal of biomaterials science. Polymer edition, 23(7), 973-990 (2011-05-10)
We prepared a novel porous gelatin (GEL) sponge which was cross-linked (CL) with a zero-length crosslinker of 2-chloro-1-methylpyridinium iodide (CMPI), and compared CPMI with 1-ethyl-3,3-dimethylaminoproplycarbodiimide (EDC). The ninhydrin assay indicated that the CMPI-CL-GEL sponge had a higher degree of cross-linking
A convenient method for the construction of β-lactam compounds from β-amino acids using 2-chloro-1-methylpyridinium iodide as condensing reagent
Huang H, et al.
Chemistry Letters (Jpn), 13(8), 1465-1466 (1984)
Jenn-Jong Young et al.
Journal of biomaterials science. Polymer edition, 15(6), 767-780 (2004-07-17)
In order to obtain much slower biodegradable films, which are often required for biomedical applications, we have developed a series of studies on heterogeneous cross-linking of hyaluronic acid (HA) films by using 2-chloro-1-methylpyridinium iodide (CMPI) or 1-ethyl-(3,3-dimethylaminopropyl)carbodiimide (EDC) as cross-linking
Dmitrii V Belykh et al.
Molecules (Basel, Switzerland), 23(7) (2018-07-18)
This article focuses on the antiradical activity of a number of 2,6-diisobornylphenol-porphyrin conjugates with various spacers between the porphyrin and phenolic fragments in the model reaction of ethylbenzene oxidation initiated by azoisobutyric acid dinitrile. The study has shown that the
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