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238252

1-碘癸烷

Name: 1-碘癸烷
Brand: ALDRICH

98%

别名:

癸基碘

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关于此项目

线性分子式:

CH₃(CH₂)₉I

化学文摘社编号:

2050-77-3

分子量:

268.18

UNSPSC Code:

12352100

NACRES:

NA.22

PubChem Substance ID:

24854150

EC Number:

218-104-1

Beilstein/REAXYS Number:

1735228

MDL number:

MFCD00001085

Assay:

98%

Form:

liquid

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属性

vapor density

>5 (vs air)

Quality Level

100

vapor pressure

0.01 mmHg ( 20 °C)

assay

98%

form

liquid

contains

copper as stabilizer

refractive index

n20/D 1.485 (lit.)

bp

132 °C/15 mmHg (lit.)

density

1.257 g/mL at 25 °C (lit.)

functional group

alkyl halide, iodo

SMILES string

CCCCCCCCCCI

InChI

1S/C10H21I/c1-2-3-4-5-6-7-8-9-10-11/h2-10H2,1H3

InChI key

SKIDNYUZJPMKFC-UHFFFAOYSA-N

说明

General description

Electrochemical reduction of 1-iododecane at mercury cathodes in DMF containing tetra-n-butylammonium perchlorate or tetramethyl ammonium perchlorate (supporting electrolyte) has been investigated.

Application

1-Iododecane has been used in the preparation of 9-nonadecanone via palladium-catalyzed carbonylative cross-coupling reaction with 9-octyl-9-borabicyclo[3.3.l]nonane.

wgk

WGK 3

pictograms

GHS07

signalword

Warning

hcodes

H315,H319,H335

pcodes

P261 - P264 - P271 - P280 - P302 + P352 - P305 + P351 + P338

Hazard Classifications

Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3

target_organs

Respiratory system

存储类别

10 - Combustible liquids

flash_point_f

230.0 °F - closed cup

flash_point_c

110 °C - closed cup

ppe

Eyeshields, Gloves, type ABEK (EN14387) respirator filter

历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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Electrochemical reduction of 1-iododecane and 1-bromodecane at a mercury cathode in dimethylformamide.

McNamee GM, et al.

Journal of the American Chemical Society, 99(6), 1831-1835 (1977)

Mono- and Bis-Alkylated Lumazine Sensitizers: Synthetic, Molecular Orbital Theory, Nucleophilic Index and Photochemical Studies.

María José Sosa et al.

Photochemistry and photobiology, 97(1), 80-90 (2020-07-07)

Mono- and bis-decylated lumazines have been synthesized and characterized. Namely, mono-decyl chain [1-decylpteridine-2,4(1,3H)-dione] 6a and bis-decyl chain [1,3-didecylpteridine-2,4(1,3H)-dione] 7a conjugates were synthesized by nucleophilic substitution (SN 2) reactions of lumazine with 1-iododecane in N,N-dimethylformamide (DMF) solvent. Decyl chain coupling occurred

Palladium-catalyzed carbonylative cross-coupling reaction of iodoalkanes with 9-alkyl-9-BBN derivatives. A direct and selective synthesis of ketones.

Ishiyama T and Miyaura N.

Tetrahedron Letters, 32(47), 6923-6926 (1991)

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全球贸易项目编号

货号	GTIN
238252-100G	04061838786746
238252-25G	04061838786753