方案
97%
表单
liquid
折射率
n20/D 1.47 (lit.)
沸点
148-150 °C/55 mmHg (lit.)
密度
1.089 g/mL at 25 °C (lit.)
应用
agriculture
environmental
SMILES字符串
CCN(CC)C(=O)CCl
InChI
1S/C6H12ClNO/c1-3-8(4-2)6(9)5-7/h3-5H2,1-2H3
InChI key
CQQUWTMMFMJEFE-UHFFFAOYSA-N
应用
2-Chloro-N,N-diethylacetamide has been used in:
- preparation of calixarene amides
- synthesis of 5-bromo-25,26,27,28-tetrakis[(N,N-diethylaminocarbonyl)-methoxy]calix[4]arene
- synthesis of amide calix[4]pyrrole macrocycles with super-extended cavities
- microwave-assisted organic synthesis of 3-cyano-N,N-diethyl-4-(4-methoxyphenoyl)-4-oxobutanamide
警示用语：
Danger
危险分类
Acute Tox. 1 Inhalation - Acute Tox. 3 Dermal - Acute Tox. 4 Oral - Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
靶器官
Respiratory system
储存分类代码
6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials
WGK
WGK 3
闪点(°F)
235.4 °F - closed cup
闪点(°C)
113 °C - closed cup
个人防护装备
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
Christopher J Woods et al.
Journal of the American Chemical Society, 124(29), 8644-8652 (2002-07-18)
A new "super-extended cavity" tetraacetylcalix[4]pyrrole derivative was synthesized and characterized, and X-ray crystal structures of complexes bound to fluoride and acetonitrile were obtained. The binding behavior of this receptor was investigated by NMR titration, and the complex was found to
Synthesis and properties of new calixarene-based ditopic receptors for the simultaneous complexation of cations and carboxylate anions.
Pelizzi N, et al.
J. Chem. Soc. Perkin Trans. II, 6, 1307-1312 (1998)
[Gas-chromatographic analysis of N,N-diethylchloracetamide in the air].
L P Shcherbakov et al.
Gigiena i sanitariia, (5)(5), 57-59 (1989-05-01)
Synthesis and crystal structures of lower rim amine and carbamoyl substituted calixarenes as transfer agents for oxyanions between an aqueous and a chloroform phase.
Wolf NJ, et al.
Polyhedron, 18(6), 855-896 (1999)
Dewei Tang et al.
Tetrahedron letters, 51(35), 4595-4598 (2010-08-07)
We herein report a dramatically improved total synthesis of the high-affinity translocator protein (TSPO) ligand DPA-714, featuring microwave-assisted organic synthesis (MAOS). Compared with previously described approaches, our novel MAOS method dramatically reduces overall reaction time without adversely effecting reaction yields.
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