301981
5,6,7,8-四氢异喹啉
95%
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关于此项目
经验公式（希尔记法）:
C9H11N
化学文摘社编号:
分子量:
133.19
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
253-098-4
MDL number:
Assay:
95%
Form:
liquid
InChI key
HTMGQIXFZMZZKD-UHFFFAOYSA-N
InChI
1S/C9H11N/c1-2-4-9-7-10-6-5-8(9)3-1/h5-7H,1-4H2
SMILES string
C1CCc2cnccc2C1
assay
95%
form
liquid
refractive index
n20/D 1.545 (lit.)
bp
106-108 °C/13 mmHg (lit.)
density
1.03 g/mL at 25 °C (lit.)
Quality Level
General description
用乙醇中的钠还原5,6,7,8-四氢异喹啉，可得到反式十氢喹啉。 5,6,7,8-四氢异喹啉也称为Bz-四氢异喹啉。
Application
5,6,7,8-四氢异喹啉被用于(±)-去氧可待因-D的全合成。 它还被用于合成7,8-二氢异喹啉-5(6H)-酮。
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
10 - Combustible liquids
wgk
WGK 3
flash_point_f
212.0 °F - closed cup
flash_point_c
100 °C - closed cup
ppe
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
Reduction of 5, 6, 7, 8-tetrahydroquinolines and 2, 3, 4, 5, 6, 7, 8, 10-octahydroquinolines to trans-decahydroquinolines.
Vierhapper FW and Eliel EL.
The Journal of Organic Chemistry, 40(19), 2734-2742 (1975)
Total synthesis of (?)-desoxycodeine-d: a novel route to the morphine skeleton.
Liou J-P and Cheng C-Y.
Tetrahedron Letters, 41(6), 915-918 (2000)
A Convenient Synthesis 7, 8-Dihydroisoquinolin-5 (6H)-One.
Lardenois P, et al.
Synthetic Communications, 26(12), 2305-2308 (1996)
Preparation of cis-and trans-Decahydroisoquinolines and of Bz-Tetrahydroisoquinoline.
Witkop B.
Journal of the American Chemical Society, 70(8), 2617-2619 (1948)
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