377112
3-吡咯啉
95%
别名:
2,5-二氢吡咯
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关于此项目
经验公式（希尔记法）:
C4H7N
化学文摘社编号:
分子量:
69.11
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
203-723-1
Beilstein/REAXYS Number:
103173
MDL number:
产品名称
3-吡咯啉, 95%
InChI key
JVQIKJMSUIMUDI-UHFFFAOYSA-N
InChI
1S/C4H7N/c1-2-4-5-3-1/h1-2,5H,3-4H2
SMILES string
C1NCC=C1
assay
95%
form
liquid
refractive index
n20/D 1.46 (lit.)
bp
90-91 °C/748 mmHg (lit.)
density
0.91 g/mL at 25 °C (lit.)
storage temp.
−20°C
Quality Level
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Application
3-吡咯啉适用于通过 X 射线光电子能谱 (XPS) 研究键合在 Si (001) 表面上的简单不饱和有机分子的核心水平结合能。它可用于合成肾素抑制剂 和血管扩张剂。
General description
3-吡咯啉是一种杂环结构单元。利用基于振动耦合模型的哈密顿模型研究了 3-吡咯啉的激发态动力学。报告了一种合成 3-吡咯啉结构单元的新方法。3-吡咯啉被报告为合成功能化吡咯啉、吡咯烷和其他天然产物的非常有用的中间体。报告了以 ( Z )-1，4-二氯-2-丁烯为原料，通过 Delépine 反应合成 3-吡咯啉（2，5-二氢-1 H -吡咯）的方法。在 N -（ 叔 -丁氧基羰基）-3-吡咯啉合成中作为中间体形成。报告了 Me 3 Al 和 Me 3 Ga 与 3-吡咯啉的反应。
通过两步烷基化/亚烷基卡宾 CH 插入反应，合成了各种 3-吡咯啉（2,5-二氢吡咯）。以 顺式 -1,4-二氯-2-丁烯为起始原料合成 3-吡咯啉。
signalword
Danger
hcodes
Hazard Classifications
Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Flam. Liq. 2 - Skin Corr. 1A
存储类别
3 - Flammable liquids
wgk
WGK 2
flash_point_f
-0.4 °F - closed cup
flash_point_c
-18 °C - closed cup
ppe
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
法规信息
危险化学品
此项目有
K Yoshino et al.
Journal of medicinal chemistry, 33(8), 2192-2196 (1990-08-01)
Structural modifications of the calcium antagonist fostedil (KB-944) and their coronary vasodilator activity are described. Amidophosphonates 4a-m, lactam amidophosphonates 7a-1, and diamide dilactam 10 were prepared, and their coronary vasodilator activity was assessed in dogs. Many compounds exhibited coronary vasodilator
An X-ray photoelectron spectroscopy study of the bonding of unsaturated organic molecules to the Si (001) surface.
Liu H and HamersRJ.
Surface Science, 416(3), 354-362 (1998)
Nobuyoshi Morita et al.
Organic letters, 6(22), 4121-4123 (2004-10-22)
[reaction: see text] The gold(III) chloride-catalyzed cycloisomerization of various alpha-aminoallenes gave the corresponding 3-pyrrolines in good to high chemical yields. An interesting dependence of the chirality transfer and reactivity on the N-protecting group was observed. The 3-pyrrolines are highly useful
Practical one-pot and large-scale synthesis of N-(tert-butyloxycarbonyl)-3-pyrroline.
Rajesh T, et al.
Organic Process Research & Development, 13(3), 638-640 (2009)
M P Green et al.
Organic letters, 3(21), 3377-3379 (2001-10-12)
[reaction: see text]. The synthesis of a range of 3-pyrrolines has been achieved from primary amine starting materials using a two-step alkylation/alkylidene carbene CH-insertion reaction sequence. We have shown that insertion into a range of CH-bond types is possible, and
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