477516
N-Boc-2,5-二氢-1H-吡咯
96%
别名:
2,5-二氢-1H-吡咯-1-羧酸叔丁酯
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关于此项目
经验公式（希尔记法）:
C9H15NO2
化学文摘社编号:
分子量:
169.22
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
MDL number:
Assay:
96%
产品名称
N-Boc-2,5-二氢-1H-吡咯, 96%
InChI
1S/C9H15NO2/c1-9(2,3)12-8(11)10-6-4-5-7-10/h4-5H,6-7H2,1-3H3
SMILES string
CC(C)(C)OC(=O)N1CC=CC1
InChI key
YEBDZDMYLQHGGZ-UHFFFAOYSA-N
assay
96%
refractive index
n20/D 1.458 (lit.)
bp
208 °C (lit.)
density
0.981 g/mL at 25 °C (lit.)
Quality Level
Application
用于与芳香重氮盐通过 Heck 芳基化反应合成 β-芳基-GABA 类似物。
N-Boc-2,5-dihydro-1H-pyrrole (tert-Butyl 2,5-dihydro-1H-pyrrole-1-carboxylate) may be used in the preparation of tert-butyl 3-aryl-2,3-dihydro-1H-pyrrole-1-carboxylate.
General description
N-Boc-2,5-dihydro-1H-pyrrole, also known as tert-butyl 2,5-dihydro-1H-pyrrole-1-carboxylate, can be synthesized from N-boc-diallylamine.
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
10 - Combustible liquids
wgk
WGK 3
flash_point_f
178.0 °F
flash_point_c
81.1 °C
ppe
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
Synthesis of aryl pyrrolizidines from endocyclic enecarbamates. Novel applications of the Heck arylation of 3-pyrrolines using diazonium salts.
de Oca ACBM and Correia CRD.
ARKIVOC (Gainesville, FL, United States), 10, 390-403 (2003)
A Short and Efficient Synthesis of (S)-1-Boc-2, 5-dihydro-1H-pyrrole-2-carboxylic Acid.
Sturmer R, et al.
Synthesis, 1, 46-48 (2001)
Ariel L L Garcia et al.
The Journal of organic chemistry, 70(3), 1050-1053 (2005-01-29)
We report herein a new, practical, and economic synthesis of the phosphodiesterase inhibitor Rolipram on a multigram scale as well as the synthesis of new 4-aryl pyrrolidones and beta-aryl-gamma-amino butyric acids (GABA derivatives) employing an efficient Heck-Matsuda arylation of 3-pyrroline
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