539430
环己酮二乙基乙缩醛
97%
别名:
1,1-二乙氧基环己烷
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关于此项目
经验公式（希尔记法）:
C10H20O2
化学文摘社编号:
分子量:
172.26
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
216-798-0
MDL number:
产品名称
环己酮二乙基乙缩醛, 97%
InChI key
MWUDABUKTZAZCX-UHFFFAOYSA-N
InChI
1S/C10H20O2/c1-3-11-10(12-4-2)8-6-5-7-9-10/h3-9H2,1-2H3
SMILES string
CCOC1(CCCCC1)OCC
assay
97%
refractive index
n20/D 1.4360 (lit.)
bp
76-78 °C/20 mmHg (lit.)
density
0.908 g/mL at 25 °C (lit.)
functional group
ether
ketal
Quality Level
Application
环己酮二乙基缩酮可用于制备 1-乙氧基环己烯。
General description
环己酮二乙基缩酮（1,1-二乙氧基环己烷）与1,3,2-苯并二恶唑硼烷[儿茶酚硼烷（CB）]反应生成相应的醚。在气相中进行热消除反应，生成1-乙氧基环己烯和乙醇。
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
3 - Flammable liquids
wgk
WGK 2
flash_point_f
140.0 °F
flash_point_c
60 °C
ppe
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
此项目有
Felix Rosas et al.
The journal of physical chemistry. A, 116(2), 846-854 (2011-12-22)
The gas-phase thermal elimination of 2,2-diethoxypropane was found to give ethanol, acetone, and ethylene, while 1,1-diethoxycyclohexane yielded 1-ethoxycyclohexene and ethanol. The kinetics determinations were carried out, with the reaction vessels deactivated with allyl bromide, and the presence of the free
Reactions of Enol Ethers with Carbenes. V. Rearrangements of Dihalocyclopropanes Derived from Six-, Seven-, and Eight-Membered Cyclic Enol Ethers1.
Parham WE, et al.
Journal of the American Chemical Society, 87(2), 321-328 (1965)
Catecholborane (1, 3, 2-benzodioxaborole). A versatile reducing agent.
Kabalka GW, et al.
The Journal of Organic Chemistry, 42(3), 512-517 (1977)
Ozonolysis-reductive amination of olefins.
Pollart KA and Miller RE.
The Journal of Organic Chemistry, 27(7), 2392-2394 (1962)
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