539430
环己酮二乙基乙缩醛
97%
别名:
1,1-二乙氧基环己烷
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关于此项目
经验公式（希尔记法）:
C10H20O2
化学文摘社编号:
分子量:
172.26
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
216-798-0
MDL number:
Assay:
97%
InChI key
MWUDABUKTZAZCX-UHFFFAOYSA-N
InChI
1S/C10H20O2/c1-3-11-10(12-4-2)8-6-5-7-9-10/h3-9H2,1-2H3
SMILES string
CCOC1(CCCCC1)OCC
assay
97%
refractive index
n20/D 1.4360 (lit.)
bp
76-78 °C/20 mmHg (lit.)
density
0.908 g/mL at 25 °C (lit.)
functional group
ether, ketal
Quality Level
General description
环己酮二乙基缩酮（1,1-二乙氧基环己烷）与1,3,2-苯并二恶唑硼烷[儿茶酚硼烷（CB）]反应生成相应的醚。在气相中进行热消除反应，生成1-乙氧基环己烯和乙醇。
Application
环己酮二乙基缩酮可用于制备 1-乙氧基环己烯。
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
3 - Flammable liquids
wgk
WGK 2
flash_point_f
140.0 °F
flash_point_c
60 °C
ppe
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
此项目有
Felix Rosas et al.
The journal of physical chemistry. A, 116(2), 846-854 (2011-12-22)
The gas-phase thermal elimination of 2,2-diethoxypropane was found to give ethanol, acetone, and ethylene, while 1,1-diethoxycyclohexane yielded 1-ethoxycyclohexene and ethanol. The kinetics determinations were carried out, with the reaction vessels deactivated with allyl bromide, and the presence of the free
Catecholborane (1, 3, 2-benzodioxaborole). A versatile reducing agent.
Kabalka GW, et al.
The Journal of Organic Chemistry, 42(3), 512-517 (1977)
Reactions of Enol Ethers with Carbenes. V. Rearrangements of Dihalocyclopropanes Derived from Six-, Seven-, and Eight-Membered Cyclic Enol Ethers1.
Parham WE, et al.
Journal of the American Chemical Society, 87(2), 321-328 (1965)
Ozonolysis-reductive amination of olefins.
Pollart KA and Miller RE.
The Journal of Organic Chemistry, 27(7), 2392-2394 (1962)
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