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Merck
CN

THS09034

H-Cube® Mini continuous flow hydrogenation reactor

AC/DC input 100 / 240 V AC

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宽度 × 高度 × 直径

217 mm × 200 mm × 250 mm

重量

6.5 kg (14.33 lb)

一般描述

  • Hydrogen is generated through electrolysis of water
  • A continuous flow of hydrogen and solvent are passed through the reactor from ambient conditions up to 100°C and 100 bar
  • When desired parameters are achieved, solvent is changed to reactant
  • The hydrogen/compound is passed through a packed column containing solid catalyst (CatCart®), where the reaction takes place
  • The product leaves the column, but the catalyst stays behind. Reductions vary in scale from 10 mg-10 g

Specifications:
  • Temperature Range: Ambient to 100°C
  • Pressure Range: 1 bar to 100 bar
  • Flow Rate: 0.1-3 mL/min
  • Hydrogen Generation: 20-25 mL/min
  • Water Reservoir Capacity: 100 mL

法律信息

CatCart is a registered trademark of ThalesNano Nanotechnology Inc.
H-Cube is a registered trademark of ThalesNano Nanotechnology Inc.

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Bruce Clapham et al.
Journal of combinatorial chemistry, 10(1), 88-93 (2007-12-22)
This manuscript details the construction of a fully automated flow hydrogenation apparatus for use in high-throughput organic synthesis. The instrument comprises of a Bohdan robot platform coupled with a ThalesNano H-cube hydrogenator and a series of solvent valves and pumping
A simple, efficient, and selective deuteration via a flow chemistry approach.
Mandity IM, Martinek TA, Darvas F, Fulop F.
Tetrahedron Letters, 50, 4372-4374 (2009)
alpha-1,4-Galacrosyltransferase-catalyzed glycosylation of sugar and lipid modified Leu-enkephalins.
Simerska P, Christie MP, Goodwin D, Jen Freda E-C, Jennings MP, Toth I.
Drug delivery, 97, 196-202 (2013)
Unexpected Inversion in the Enantioselective Hydrogenation of 2,2,2-Trifluoroacetophenone on Pt-Cinchona Chiral Catalyst Using Continuous-Flow Fixed-Bed Reactor.
Szollosi Gy; Cserenyi Sz; Bartok M.
Catalysis Letters, 134, 264-269 (2010)
Synthesis of an azabicyclic framework towards (?)-actinophyllic acid.
Mortimer D, Whiting M, Harrity JPA, Jones S, Coldham I.
Tetrahedron Letters, 55, 1255-1257 (2014)
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