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Merck
CN

B-004

苯甲酰芽子碱标准液 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

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经验公式（希尔记法）:
C16H19NO4
化学文摘社编号:
519-09-5
分子量:
289.33
NACRES:
NA.24
PubChem Substance ID:
329773092
UNSPSC Code:
41116107
MDL number:
MFCD00070263

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InChI key

GVGYEFKIHJTNQZ-RFQIPJPRSA-N

SMILES string

CN1[C@H]2CC[C@@H]1[C@H]([C@H](C2)OC(=O)c3ccccc3)C(O)=O

InChI

1S/C16H19NO4/c1-17-11-7-8-12(17)14(15(18)19)13(9-11)21-16(20)10-5-3-2-4-6-10/h2-6,11-14H,7-9H2,1H3,(H,18,19)/t11-,12+,13-,14+/m0/s1

grade

certified reference material

form

liquid

feature

SNAP-N-SPIKE®, SNAP-N-SHOOT®

packaging

ampule of 1 mL

manufacturer/tradename

Cerilliant®

drug control

Narcotic Licence Schedule A (Switzerland); estupefaciente (Spain); Decreto Lei 15/93: Tabela IB (Portugal), kontrollierte Droge in Deutschland

Quality Level

300

concentration

1.0 mg/mL in methanol

technique(s)

gas chromatography (GC): suitable, liquid chromatography (LC): suitable

application(s)

forensics and toxicology

format

single component solution

shipped in

wet ice

storage temp.

−20°C

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General description

该认证参考标准品适用于各种 LC/MS 或 GC/MS 应用，包括从法医分析和临床毒理学到尿液药物测试。

苯甲酰爱康宁是可卡因的初级代谢产物，也是确定吸食可卡因的主要生物标记物。苯甲酰爱康宁也是处方药 Esterom 中的主要药物成分，Esterom 是一种局部镇痛药，用于缓解肌肉疼痛。

Application

该认证参考溶液（CRM)也可用于以下应用：
  • 开发和确认用于测定115份收缴样品中可卡因产品的可卡因、两种主要降解产物以及常见掺杂剂的高效液相色谱-二极管阵列检测器（HPLC-DAD）方法
  • 采用整体分子印迹聚合物（MIP）固相微萃取（SPME）和之后的紫外检测分析人尿样品中的苯甲酰爱康宁
  • 通过疏水相互作用-串联质谱法（HILIC-MS/MS）分离和测定头发样品中的可卡因及其代谢产物― 苯甲酰爱康宁、芽子碱甲酯和可卡乙碱
  • 通过超高效液相色谱-串联质谱法（UHPLC-MS/MS）评估干血斑（DBS）中的可卡因、苯甲酰爱康宁、 可卡乙碱、芽子碱甲酯（EME）和去甲可卡因
  • 通过超高压液相色谱--电喷雾电离（UPLC-ESI）和三重四极杆串联质谱进行尸体血样中甲苯噻嗪、游离吗啡、6 -乙酰吗啡、可待因、可卡因和苯甲酰爱康宁的多残留分析。

Features and Benefits

  • 经ISO/IEC 17025 和ISO 17034认证进行全面表征
  • 随附全面的分析证书（CoA），标明稳定性、均匀性、浓度准确性、不确定性和可追溯性
  • 通过实时稳定性研究进行严格测试以确保准确性和有效期
  • 采用确认合规的精密天平以重力测定法制备，以确保最低的不确定性
  • 装入安瓿并在氩气氛围下火焰密封以确保长有效期
  • 以便捷、DEA赦免的形式提供以提高实验室效率

Legal Information

German
Dieses Produkt fällt unter das Betäubungsmittelgesetz (BtMG). Für eine Bestellung dieses Produktes ist eine Erlaubnis nach § 3 BtMG zwingend erforderlich, es sei denn, es greift eine Ausnahme von der Erlaubnispflicht nach § 4 oder § 26 BtMG.

English
This product is subject to the German Narcotics Act. A permit under Section 3 of the German Narcotics Act is mandatory for ordering this product unless an exemption from the permit requirement under Section 4 or Section 26 of the German Narcotics Act applies.
CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany
Snap-N-Shoot is a registered trademark of Cerilliant Corporation
Snap-N-Spike is a registered trademark of Merck KGaA, Darmstadt, Germany

signalword

Danger

Hazard Classifications

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Flam. Liq. 2 - STOT SE 1

target_organs

Eyes,Central nervous system

存储类别

3 - Flammable liquids

wgk

WGK 2

flash_point_f

49.5 °F - closed cup

flash_point_c

9.7 °C - closed cup

法规信息

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Thomas Bouvarel et al.
Talanta, 233, 122611-122611 (2021-07-04)
A simple, selective, and sensitive method involving a miniaturized solid phase extraction step based on a monolithic molecularly imprinted polymer (MIP) directly coupled on-line to UV detection was developed for the determination of benzoylecgonine (BZE) in complex biological samples. Monolithic
Sara Castiglioni et al.
Environmental science & technology, 47(3), 1452-1460 (2012-12-25)
The aim of this study was to integrally address the uncertainty associated with all the steps used to estimate community drug consumption through the chemical analysis of sewage biomarkers of illicit drugs. Uncertainty has been evaluated for sampling, chemical analysis
Nadine Schaefer et al.
Analytical and bioanalytical chemistry, 405(1), 247-258 (2012-10-19)
In the context of driving ability diagnostics in Germany, administrative cutoffs for various drugs and pharmaceuticals in urine have been established. Two liquid chromatography-tandem mass spectrometry methods for simultaneous detection and quantification of amphetamines, designer amphetamines, benzoylecgonine, benzodiazepines, opiates, and
Charles A Dackis et al.
Journal of substance abuse treatment, 43(3), 303-312 (2012-03-02)
This is a randomized, double-blind, placebo-controlled study of modafinil treatment for cocaine dependence. Patients (N = 210) who were actively using cocaine at baseline were randomized to 8 weeks of modafinil (0 mg/day, 200 mg/day, or 400 mg/day) combined with
Lubertus Bijlsma et al.
The Science of the total environment, 443, 200-208 (2012-11-29)
In this work, ultra-high-performance liquid chromatography (UHPLC) coupled to a hybrid quadrupole time-of-flight mass spectrometer (QTOF MS) has allowed the discovery and elucidation of degradation products of cocaine and its main metabolite benzoylecgonine (BE) in water. Spiked surface water was
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