8.52052
Fmoc-His(Boc)-OH-CHA
Novabiochem®
别名:
Fmoc-His(Boc)-OH-CHA, N-α-Fmoc-N-im-t.-Boc-L-histidine cyclohexylammonium salt
产品线
Novabiochem®
方案
≥97% (TLC)
≥97.0% (HPLC)
表单
powder
反应适用性
reaction type: Fmoc solid-phase peptide synthesis
制造商/商品名称
Novabiochem®
应用
peptide synthesis
官能团
Boc
Fmoc
储存温度
−20°C (−15°C to −25°C)
InChI
1S/C26H27N3O6.C6H13N/c1-26(2,3)35-25(33)29-13-16(27-15-29)12-22(23(30)31)28-24(32)34-14-21-19-10-6-4-8-17(19)18-9-5-7-11-20(18)21;7-6-4-2-1-3-5-6/h4-11,13,15,21-22H,12,14H2,1-3H3,(H,28,32)(H,30,31);6H,1-5,7H2/t22-;/m0./s1
InChI key
UDEXYAHZNOKVIG-FTBISJDPSA-N
一般描述
The N-im-Boc group is unstable to prolonged treatment with piperidine [1]; the utility of this derivative is therefore limited to the preparation of short sequences by Fmoc SPPS. This derivative is supplied as a CHA-salt.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Fmoc SPPS
Literature references
[1] P. Sieber, et al. (1987) Tetrahedron Lett., 28, 6031.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Fmoc SPPS
Literature references
[1] P. Sieber, et al. (1987) Tetrahedron Lett., 28, 6031.
分析说明
Color (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Enantiomeric purity: ≥ 99.5 % (a/a)
Purity (TLC(011A)): ≥ 97 %
Purity (TLC(157B)): ≥ 97 %
Assay (HPLC, area%): ≥ 97.0 % (a/a)
Water (K. F.): ≤ 1.00 %
To see the solvent systems used for TLC of Novabiochem® products please click here.
Appearance of substance (visual): powder
Identity (IR): passes test
Enantiomeric purity: ≥ 99.5 % (a/a)
Purity (TLC(011A)): ≥ 97 %
Purity (TLC(157B)): ≥ 97 %
Assay (HPLC, area%): ≥ 97.0 % (a/a)
Water (K. F.): ≤ 1.00 %
To see the solvent systems used for TLC of Novabiochem® products please click here.
其他说明
Replaces: 04-12-1110
法律信息
Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany
储存分类代码
11 - Combustible Solids
WGK
WGK 2
闪点(°C)
Not applicable
法规信息
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