DX1726
N,N-二甲基甲酰胺
OmniSolv®
别名:
DMF, NSC 5356
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关于此项目
线性分子式:
HCON(CH3)2
化学文摘社编号:
分子量:
73.09
EC Index Number:
200-679-5
UNSPSC Code:
12352111
Beilstein/REAXYS Number:
605365
MDL number:
Assay:
≥99.9% (GC)
Technique(s):
HPLC: suitable
LC/MS: suitable
gas chromatography (GC): suitable
LC/MS: suitable
gas chromatography (GC): suitable
Bp:
153 °C (lit.)
Vapor pressure:
2.7 mmHg ( 20 °C)
产品名称
N,N-二甲基甲酰胺, OmniSolv®
SMILES string
[H]C(=O)N(C)C
InChI key
ZMXDDKWLCZADIW-UHFFFAOYSA-N
InChI
1S/C3H7NO/c1-4(2)3-5/h3H,1-2H3
vapor density
2.5 (vs air)
vapor pressure
2.7 mmHg ( 20 °C)
product line
OmniSolv®
assay
≥99.9% (GC)
form
liquid
autoignition temp.
833 °F
shelf life
24 mo.
expl. lim.
15.2 %
technique(s)
HPLC: suitable
LC/MS: suitable
gas chromatography (GC): suitable
impurities
<0.05% Water
evapn. residue
<5 ppm
color
APHA: 10
refractive index
n20/D 1.430 (lit.)
pH
7 (20 °C, 200 g/L in H2O)
bp
153 °C (lit.)
mp
−61 °C (lit.)
transition temp
flash point 57.5 °C
density
0.944 g/mL (lit.)
UV cutoff
≤268 nm
UV absorption
λ: 268 nm Amax: ≤1.00
λ: 270 nm Amax: ≤0.75
λ: 275 nm Amax: ≤0.30
λ: 295 nm Amax: ≤0.07
λ: 310 nm Amax: ≤0.03
λ: 340 nm Amax: ≤0.01
shipped in
ambient
storage temp.
room temp
Quality Level
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Application
多种疏水性有机化合物的溶剂。
N,N-Dimethylformamide (DMF) is used
- As a solvent in the Wittig reaction for synthesizing α-hydroxy amides.
- In the preparation of the Vilsmeier reagent when treated with phosphorus oxychloride or other acid chlorides, which is utilized for formylating, halogenating, and dehydroxylating reactions.
- As a solvent in the synthesis of alkyl halides from alcohols.
- As a co-solvent to examine the relationship between medium polarity and drug solubility.
OmniSolv®
Analysis Note
Assay (GC): 99.9% min
Color (APHA): 10 max
Evaporation residue: 5ppm max
Expiration date: 24 months
Filtered through 0.2 m filter: To pass test
Form: Clear liquid
Infrared Spectrum: Conforms to standard
Titrable acid: eq/g
Titrable base: eq/g
UV Abs. at 268 nm: 1.00AU max
UV Abs. at 270 nm: 0.75AU max
UV Abs. at 275 nm: 0.30AU max
UV Abs. at 295 nm: 0.07AU max
UV Abs. at 310 nm: 0.03AU max
UV Abs. at 340 nm: 0.01AU max
UV Cut-off: 268nm max
Water (H2O): 0.05% max
Color (APHA): 10 max
Evaporation residue: 5ppm max
Expiration date: 24 months
Filtered through 0.2 m filter: To pass test
Form: Clear liquid
Infrared Spectrum: Conforms to standard
Titrable acid: eq/g
Titrable base: eq/g
UV Abs. at 268 nm: 1.00AU max
UV Abs. at 270 nm: 0.75AU max
UV Abs. at 275 nm: 0.30AU max
UV Abs. at 295 nm: 0.07AU max
UV Abs. at 310 nm: 0.03AU max
UV Abs. at 340 nm: 0.01AU max
UV Cut-off: 268nm max
Water (H2O): 0.05% max
General description
N,N - Dimethylformamide (DMF) is a highly effective polar aprotic solvent for a wide range of compounds. This is due to its ability to interact effectively with different compounds. DMF can function as both an electrophilic and nucleophilic agent, and it can provide various key intermediates that mediate chemical reactions.
Packaging
M-Bottle for Solvents
As a global leader in lab reagents, we are constantly looking for new ways to optimize the safety of our products. The newly developed 4L solvent bottle design features advanced sealing technology that eliminates leaks to make the handling of solvents safer and more convenient than ever before.
See all the new features here!
As a global leader in lab reagents, we are constantly looking for new ways to optimize the safety of our products. The newly developed 4L solvent bottle design features advanced sealing technology that eliminates leaks to make the handling of solvents safer and more convenient than ever before.
See all the new features here!
is packaged in 1L amber glass bottle
is packaged in 4L amber glass bottle
is packaged in 4L polycoated glass bottle
Preparation Note
Product filtered through a 0.2 μm filter
Legal Information
OMNISOLV is a registered trademark of Merck KGaA, Darmstadt, Germany
signalword
Danger
Hazard Classifications
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Eye Irrit. 2 - Flam. Liq. 3 - Repr. 1B
存储类别
3 - Flammable liquids
wgk
WGK 2
flash_point_f
135.5 °F - closed cup
flash_point_c
57.5 °C - closed cup
法规信息
新产品
此项目有
Phenformin in aqueous co-solvent mixtures of N, N-dimethylformamide, ethanol, N-methylpyrrolidone and dimethyl sulfoxide: Solubility, solvent effect and preferential solvation
Zhao, Xi and Farajtabar, et. al.
The Journal of Chemical Thermodynamics, 144, 106085-106085 (2020)
N, N-Dimethylformamide: much more than a solvent
Muzart, Jacques
Tetrahedron, 65, 8313-8323 (2009)
Formation of poly (vinylidene fluoride) crystalline phases from tetrahydrofuran/N, N-dimethylformamide mixed solvent}
Ma, Wenzhong and Zhang, Jun and Wang, Xiaolin
Journal of Materials Science, 43, 398-401 (2008)
N, N-Dimethylformamide
Comins, Daniel L and Joseph, Sajan P
Encyclopedia of Reagents for Organic Synthesis, Second Edition (2001)
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