92337
溴三甲基硅烷
purum, ≥97.0% (AT)
别名:
TMBS, 三甲基溴化硅, 三甲基溴硅烷
等级
purum
质量水平
方案
≥97.0% (AT)
表单
liquid
包含
silver wool as stabilizer
折射率
n20/D 1.424 (lit.)
n20/D 1.424
沸点
79 °C (lit.)
密度
1.16 g/mL at 25 °C (lit.)
储存温度
2-8°C
SMILES字符串
C[Si](C)(C)Br
InChI
1S/C3H9BrSi/c1-5(2,3)4/h1-3H3
InChI key
IYYIVELXUANFED-UHFFFAOYSA-N
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一般描述
三甲基溴硅烷可与Cl3共同用于催化烯丙基三甲基硅烷对各种醇的直接烯丙基化。
应用
三甲基溴硅烷可作为衍生化试剂，用于通过气相色谱技术测定细胞培养基中的烷化溶血磷脂。
其他说明
强效甲硅烷基化试剂；用于醚的裂解；以及膦酸和磷酸烷基酯的平稳裂解
警示用语：
Danger
危险分类
Aquatic Acute 1 - Aquatic Chronic 1 - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1B - STOT SE 3
靶器官
Respiratory system
补充剂危害
储存分类代码
3 - Flammable liquids
WGK
WGK 3
闪点(°F)
10.4 °F - closed cup
闪点(°C)
-12 °C - closed cup
个人防护装备
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
法规信息
危险化学品
此项目有
C. Flann et al.
Journal of the American Chemical Society, 109, 6097-6097 (1987)
J. Heberle et al.
Silylating Agents, 2nd ed. (1995)
J.L. Meek et al.
Journal of the American Chemical Society, 110, 2317-2317 (1988)
S. Hanessian et al.
Tetrahedron Letters, 25, 2515-2515 (1984)
Catherine Taillier et al.
Organic letters, 6(13), 2149-2151 (2004-06-18)
[reaction: see text] (+)-Zoapatanol was synthesized by using four key-steps: a Suzuki cross-coupling to prepare a (Z)-alpha,beta-unsaturated ester followed by an enantioselective dihydroxylation to control the C2' and C3' stereocenters, an intramolecular Horner-Wadsworth-Emmons olefination to construct the oxepane ring, and
商品
Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs
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