Merck
CN

23184

Sigma-Aldrich

氯甲酸-9-芴基甲酯

BioReagent, ≥99.0% (HPLC)

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别名:
9-芴甲氧羰酰氯, Fmoc-Cl, 芴甲氧羰酰氯
Empirical Formula (Hill Notation):
C15H11ClO2
CAS号:
分子量:
258.70
Beilstein:
2279177
EC 号:
MDL编号:
PubChem化学物质编号:

产品线

BioReagent

质量水平

检测方案

≥99.0% (HPLC)

形式

solid

mp

61-64 °C
62-64 °C (lit.)

官能团

Fmoc

储存温度

2-8°C

SMILES string

ClC(=O)OCC1c2ccccc2-c3ccccc13

InChI

1S/C15H11ClO2/c16-15(17)18-9-14-12-7-3-1-5-10(12)11-6-2-4-8-13(11)14/h1-8,14H,9H2

InChI key

IRXSLJNXXZKURP-UHFFFAOYSA-N

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此商品
160512469208.52259
Fmoc chloride BioReagent, ≥99.0% (HPLC)

Sigma-Aldrich

23184

氯甲酸-9-芴基甲酯

Fmoc chloride 97%

Sigma-Aldrich

160512

氯甲酸-9-芴基甲酯

assay

≥99.0% (HPLC)

assay

97%

assay

≥98.0% (HPLC)

assay

≥98.0% (HPLC)

form

solid

form

solid

form

powder

form

powder

mp

61-64 °C, 62-64 °C (lit.)

mp

62-64 °C (lit.)

mp

150-153 °C (lit.)

mp

60-63 °C

functional group

Fmoc

functional group

Fmoc

functional group

Fmoc

functional group

-

storage temp.

2-8°C

storage temp.

2-8°C

storage temp.

2-8°C

storage temp.

2-8°C

应用

9-芴甲氧基碳酰氯(Fmoc-Cl)是用于氨基酸和生物胺的柱前衍生化的试剂,用于HPLC氨基酸分析以及制备用于固相肽合成的N-Fmoc氨基酸。
在氨基酸 HPLC 分析中,用于衍生化氨基酸;在固相肽合成中用于制备 N-Fmoc 氨基酸。

其他说明

用作氨基酸柱前荧光衍生化的试剂

象形图

Corrosion

警示用语:

Danger

危险声明

危险分类

Eye Dam. 1 - Skin Corr. 1B

补充剂危害

储存分类代码

8A - Combustible, corrosive hazardous materials

WGK

WGK 3

闪点(°F)

Not applicable

闪点(°C)

Not applicable

个人防护装备

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges


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Phthaldialdehyde suitable for HPLC fluorimetric detection of amino acids, ≥99% (HPLC), powder or crystals

Sigma-Aldrich

P0657

邻苯二甲醛

P Fürst et al.
Journal of chromatography, 499, 557-569 (1990-01-19)
Reversed-phase high-performance liquid chromatography (RP-HPLC) is a powerful method for assaying physiological amino acid concentrations in biological fluids. Four pre-column derivatization methods, with o-phthaldialdehyde (OPA), 9-fluorenylmethyl chloroformate (FMOC-Cl), phenyl isothiocyanate (PITC) and 1-dimethylaminonaphthalene-5-sulphonyl chloride (dansyl-Cl), were assessed with respect to
A Jámbor et al.
Journal of chromatography. A, 1216(34), 6218-6223 (2009-07-28)
This paper, as a novelty to this field, presents the deproteinization and derivatization of plasma's free amino acids (PFAAs), simultaneously, in a single step, with the acetonitrile (ACN) containing 9-fluorenylmethyloxycarbonyl chloride (FMOC) reagent. Deproteinization and derivatization, were studied with 22
Valentin Lozanov et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 860(1), 92-97 (2007-11-07)
A liquid chromatography method for simultaneous analysis of amino acids, polyamines, catecholeamines and metanephrines in human body fluids after derivatization with 9-fluorenylmethyloxycarbonyl chloride was developed. The chromatographic behavior of analytes at different pH of mobile phase was studied. Successful baseline
E J Miller et al.
Analytical biochemistry, 190(1), 92-97 (1990-10-01)
A recently described procedure for amino acid analyses has been modified and adapted for use in quantitating the unique mixture of products commonly found in hydrolysates of the collagens. The method involves precolumn derivatization of hydrolysates with 9-fluorenylmethyl chloroformate (FMOC-CL)
Ibolya Molnár-Perl
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 879(17-18), 1241-1269 (2011-03-05)
An overview is presented on the advancement of the two most frequently used derivatization protocols applying the o-phthalaldehyde (OPA)-thiol and the fluorenylmethyloxycarbonyl (FMOC) chloride reagents, prior to the high performance liquid chromatographic analysis of amino acids. This review pays special

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