Merck
CN

39220

Sigma-Aldrich

丹磺酰氯

BioReagent, suitable for fluorescence, ≥99.0% (HPLC)

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别名:
1-二甲基氨基萘-5-磺酰氯, 5-(二甲基氨基)萘-1-磺酰氯, DNSCl, 氯化二硝基水杨酸, 5-(二甲基氨基)-萘-1-磺酰氯
经验公式(希尔记法):
C12H12ClNO2S
CAS号:
分子量:
269.75
Beilstein:
2217205
EC 号:
MDL编号:
PubChem化学物质编号:
NACRES:
NA.32

产品线

BioReagent

质量水平

检测方案

≥99.0% (HPLC)

mp

72-74 °C (lit.)

溶解性

acetone: 0.2 g/10 mL

荧光

λex 337 nm; λem 492 nm in chloroform (after derivatization with hexylamine)

适用性

suitable for fluorescence

储存温度

2-8°C

SMILES字符串

CN(C)c1cccc2c(cccc12)S(Cl)(=O)=O

InChI

1S/C12H12ClNO2S/c1-14(2)11-7-3-6-10-9(11)5-4-8-12(10)17(13,15)16/h3-8H,1-2H3

InChI key

XPDXVDYUQZHFPV-UHFFFAOYSA-N

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相关类别

一般描述

丹磺酰氯又称5-二甲基氨基萘-1-磺酰氯,是一种柱前衍生化试剂。 衍生化反应后,荧光衍生物可使用NMR、IR、UV-vis和荧光显微镜等多种分析方法分析。丹磺酰氯是一种典型的芳香族磺酰氯,它与各种碱反应,生成具有不同稳定性的衍生物。

应用

丹磺酰氯用作衍生化试剂,用于临床前研究研究乙炔雌二醇的大量代谢和最低给药剂量。 使用丹磺酰氯获得衍生物通过HPLC方法测定人血清中双酚的研究。 丹磺酰氯衍生物适用于LC/MS测定和表征食品样品中草甘膦、氨甲基膦酸(AMPA)和草铵膦 。
一种用于氨基酸和肽的荧光N-末端衍生化的荧光试剂,并且可用反相HPLC进行检测。

象形图

Corrosion

警示用语:

Danger

危险声明

危险分类

Eye Dam. 1 - Met. Corr. 1 - Skin Corr. 1B

储存分类代码

8A - Combustible, corrosive hazardous materials

WGK

WGK 3

个人防护装备

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges


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Martins Jansons et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 1177, 122779-122779 (2021-06-08)
Glyphosate and other polar and acidic pesticides have been particularly studied due to the concerns over widespread and intensive use. The chemical properties of these compounds necessitate use of customised methods, such as derivatisation or ion exchange chromatography. These approaches
Sarah A Goretta et al.
Bioorganic & medicinal chemistry, 20(13), 4012-4019 (2012-06-08)
Sphingomyelin (SM) and cholesterol form microdomains called lipid rafts in cellular membranes. To develop a versatile fluorescent lipid probe, chemical modifications to both the hydrophobic and hydrophilic portions of SM are essential. Few reports describing SM probes with a fluorophore
Cuicui Guo et al.
Journal of separation science, 44(16), 3052-3060 (2021-06-09)
Human exposure to bisphenols has rarely been reported. The most important challenges in this regard are the sensitivity and accuracy of the analytical methods employed. Dansyl chloride derivatization prior to high-performance liquid chromatography-tandem mass spectrometry has been prevalently employed to
Shaodong Jia et al.
Journal of chromatography. A, 1218(51), 9174-9182 (2011-11-15)
A novel liquid chromatography coupled with quadrupole time-of-flight mass spectrometry (LC-Q-TOFMS) method was developed for the simultaneous determination of 23 amino acids and 7 biogenic amines in food samples. These analytes were pre-column derivatized with dansyl chloride and then separated
Balaraman H Shankar et al.
The journal of physical chemistry. B, 115(45), 13292-13299 (2011-10-11)
Interaction of a few dansyl-naphthalimide conjugates 1a-e linked through polymethylene spacer groups with various metal ions was investigated through absorption, fluorescence, NMR, isothermal calorimetric (ITC), and laser flash photolysis techniques. The characteristic feature of these dyads is that they exhibit

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