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Merck
CN

24050

SPB®-5毛细管GC色谱柱

L × I.D. 60 m × 0.32 mm, df 0.25 μm

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eCl@ss:
32119290
UNSPSC Code:
41115710
NACRES:
SB.54
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material

fused silica

agency

meets requirements for USP G27 and G36

parameter

-60-320 °C temperature (isothermal or programmed)

Beta value

320

df

0.25 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

60 m × 0.32 mm

matrix active group

SPB 5, Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

column type

capillary non-polar

General description

应用:这种非极性通用色谱柱主要使得组份按照沸点高低顺序洗脱,选择性略有提高,特别适用于芳香族化合物。
USP 代码:本色谱柱符合 USP G27 和 G36 要求。

  • 结合的
  • 聚(5% 二苯基/ 95% 二甲基硅氧烷)
温度限制
  • ≤0.32mm 内径,<2 μm:-60°C 至 320°C(等温或程序化)
  • ≤0.32mm 内径,<2 μm:-60°C 至 300°C(等温或程序化)
  • ≥0.53mm 内径,<2 μm:-60°C 至 300°C(等温)或 320°C(程序化)
  • ≥0.53mm 内径,<2 μm:-60°C 至 260°C(等温)或 280°C(程序化)

Application

SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may also be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. Furthermore, it may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany


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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
Zhihua Fan et al.
Environmental science & technology, 40(19), 6051-6057 (2006-10-21)
A sensitive, simple, and cost-effective passive sampling methodology was developed to quantify personal exposure to gaseous polycyclic aromatic hydrocarbons (PAHs). A Fan-Lioy passive PAH sampler (FL-PPS) is constructed from 320 sections of 1-cm long SPB-5 GC columns (0.75-mm i.d. and
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave



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