material
fused silica
Quality Level
agency
meets requirements for USP G27 and G36
parameter
-60-300 °C temperature (isothermal), -60-320 °C temperature (programmed)
Beta value
133
df
1.00 μm
technique(s)
gas chromatography (GC): suitable
L × I.D.
30 m × 0.53 mm
matrix active group
SPB 5, Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase
column type
capillary non-polar
General description
毛细管GC柱也称开口管柱。载气流过中心孔,并且在整个柱长上不受限制。
应用:这种非极性通用色谱柱主要使得组份按照沸点高低顺序洗脱,选择性略有提高,特别适用于芳香族化合物。
USP 代码:本色谱柱符合 USP G27 和 G36 要求。
相:
USP 代码:本色谱柱符合 USP G27 和 G36 要求。
相:
- 结合的
- 聚(5% 二苯基/ 95% 二甲基硅氧烷)
- ≤0.32mm 内径,<2 μm:-60°C 至 320°C(等温或程序化)
- ≤0.32mm 内径,<2 μm:-60°C 至 300°C(等温或程序化)
- ≥0.53mm 内径,<2 μm:-60°C 至 300°C(等温)或 320°C(程序化)
- ≥0.53mm 内径,<2 μm:-60°C 至 260°C(等温)或 280°C(程序化)
Application
SPB®-5毛细管气相色谱柱可作为电子捕获气相色谱法测定谷物中雪腐镰刀菌烯醇和脱氧雪腐镰刀菌烯醇的固定相。
Other Notes
我们提供多种色谱配件,包括分析进样针
Legal Information
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
Determination of sterols by capillary column gas chromatography. Differentiation among different types of olive oil: virgin, refined, and solvent-extracted.
Jimenez O and Gonzalez ADV.
Journal of the American Oil Chemists' Society, 73 (12), 1685-1689 (1996)
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