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55227-U

Supel QuE QuEChERS tube

Citrate Extraction Tube, pk of 50, suitable for EN 15662

别名:

QuEChERS

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关于此项目

UNSPSC Code:
41115712
NACRES:
NB.21
Material:
polypropylene tube
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产品名称

Supel QuE, Citrate Extraction Tube, pk of 50, suitable for EN 15662

material

polypropylene tube

Quality Level

agency

suitable for EN 15662

product line

Supel

composition

magnesium sulfate, 4 g , sodium chloride, 1 g (Cat. No. S7653), sodium citrate dibasic sesquihydrate, 0.5 g (Cat. No. 71635), sodium citrate tribasic dihydrate, 1 g (Cat. No. S4641)

packaging

pk of 50

technique(s)

QuEChERS: suitable

centrifuge tube volume

15 mL

application(s)

food and beverages

separation technique

ion exchange

General description

分散SPE法,通常也是指"QuEChERS” 方法(快速,简便,便宜,有效,耐用和安全),是一种现代样本准备技术,正在越来越多地被用在食品和农业产品多残基杀虫剂分析领域。

使用QuEChERS方法,食品/农产品样本首先在水溶性溶剂(比如乙腈),在高盐(比如氯化钠和硫酸镁)和或者缓冲试剂(比如柠檬酸盐)存在下,进行提取。高盐能够引起液相分离,而缓冲试剂能够稳定酸碱不稳定杀虫剂。 在摇晃和离心之后,有机相部分就进一步用SPE清洁。 和传统的SPE管方法不同,在分散SPE中,清洁需要混合大量的SPE(比如Supelclean PSA, ENVI-Carb, 和或者Discovery DSC-18)和提取物。 在样本清洁后,混合物经过离心,得到的上清可以直接分析,或者在分析前需要很少的处理。

Supelco有一系列的管和离心管,含有预置量的盐和SPE吸附剂,能够支持现今最常用的方法。

Application

Supel QuE柠檬酸盐小柱用于通过各种分析技术测定蔬菜上的农残。
适用于提取约10 g食品/农业样品。 柠檬酸盐用于缓冲萃取至pH 5.0-5.5。 在该pH下,大多数酸碱不稳定农药可保持稳定。

Legal Information

Supel is a trademark of Sigma-Aldrich Co. LLC


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存储类别

13 - Non Combustible Solids

wgk

WGK 1

flash_point_f

Not applicable

flash_point_c

Not applicable



历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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实验方案

Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.

商品

2-layer SPE cartridge efficiently reduces background for ginger contaminant analysis.

Pistachios 45% fat complicates pesticide analysis. But Z-Sep+ sorbent cleanup after QuEChERS extraction can reduce background for reliable results.

SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.

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相关内容

QuEChERS is a ‘Quick, Easy, Cheap, Effective, Rugged and Safe’ sample cleanup method used to prepare food and agricultural samples for pesticides analysis. QuEChERS is based on the Solid Phase Extraction (SPE) technique of sample preparation.

固相萃取(SPE)是一种用在色谱分析(如 HPLC、GC、TLC 色谱)前快速、选择性制备和纯化样品的技术,主要用于置换样品基质、浓缩分析物、去除干扰成分和污染物,以改善数据结果、保护分析色谱柱。

Solid phase extraction purifies samples for chromatographic analysis, improving data quality and protecting analytical columns.


Monitoring survey of the use patterns and pesticide residues on vegetables in the Niayes zone, Senegal
Diop A, et al.
Chemosphere, 144, 1715-1721 (2016)
Pesticide analysis at ppt concentration levels: coupling nano-liquid chromatography with dielectric barrier discharge ionization-mass spectrometry
Mirabelli.FM, et al.
Analytical and Bioanalytical Chemistry, 408(13), 3425-3434 (2016)
Maria Teresa Salles Trevisan et al.
Journal of chromatography. A, 1512, 98-106 (2017-07-20)
An analytical method using a quick, easy, cheap, effective, rugged and safe (QuEChERS) procedure for multi-residue determination of 52 pesticides in coffee leaf extractshas been developed and validated according to SANTE/11945/2015 guidelines. Different sorbent combinations for dispersive solid phase extraction



全球贸易项目编号

货号GTIN
55227-U04061835552382