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About This Item
product line
KitAlysis™
reaction suitability
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
functional group
phosphine
Application
Step-by-Step Guide for KitAlysis High-Throughput Base Reaction Screening Kit
Downloadable experimental excel file
Each kit contains 2 customizable screening sets that contain the following:
- 7 X 2 pre-weighed bases (30 μmol) in individual microvials with magnetic stir bars
- 4 X 2 base solutions
- 2 empty microvials for Chemist′s Choice of base allowing customization
- 4 degassed anhydrous solvents (DMF, MeOH, THF, Toluene)
- 2 NEW KitAlysis 24-Well Reaction Block Replacement Films
- 4 empty substrate stock solution reaction vials with stirbars
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
Features and Benefits
- Designed and tested by synthetic chemists
- Easily run 24-microscale reactions in parallel
- 10 μmol reactions with 3 equiv. base, 0.1 M concentration
- Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks
Legal Information
Kit Components Only
- Potassium bicarbonate, ACS reagent, 99.7%, powder, crystals or granules
Kit Components Also Available Separately
- RDD019Potassium phosphate tribasic, anhydrous, free-flowing, Redi-Dri™, reagent grade, ≥97%
- 441902Cesium carbonate, ReagentPlus®, 99%
- 757551Potassium hydroxide, ≥99.95% trace metals basis
- 791733Potassium acetate, anhydrous, free-flowing, Redi-Dri™, ACS reagent, ≥99.0%
- 1390091,8-Diazabicyclo[5.4.0]undec-7-ene, 98%
- 225770Lithium bis(trimethylsilyl)amide solution, 1.0 M in THF
- 702706Sodium tert-butoxide solution, 2 M in THF, ZerO2®
- 900522Toluene, anhydrous, ZerO2®, 99.8%
- 900632Triethylamine, ZerO2®, ≥99%
- 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9%
- 900638N,N-Dimethylformamide, anhydrous, ZerO2®, 99.8%
- 900641Methanol, anhydrous, ZerO2®, 99.8%
- Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm
- Z742110KitAlysis™ 24-well reaction block replacement film
- 900501Potassium carbonate, anhydrous, free-flowing, Redi-Dri™, ReagentPlus®, 99%
- 655104Sodium hydroxide, reagent grade, 97%, powder
Signal Word
Danger
Hazard Statements
Precautionary Statements
Hazard Classifications
Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 2 - STOT RE 2 Oral
Target Organs
Kidney,Adrenal gland,Testes
Supplementary Hazards
Storage Class Code
4.1B - Flammable solid hazardous materials
Flash Point(F)
-5.8 °F
Flash Point(C)
-21 °C
Regulatory Information
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Articles
KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
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Instructions
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