8.53018
Boc-Lys(2-Cl-Z)-OH
(cryst) Novabiochem®
Synonym(s):
Boc-Lys(2-Cl-Z)-OH, N-α-t.-Boc-N-ε-2-chloro-CBZ-L-lysine
Select a Size
About This Item
Quality Level
product line
Novabiochem®
assay
≥95.0% (acidimetric), ≥98% (TLC), ≥99.0% (HPLC)
form
powder
reaction suitability
reaction type: Boc solid-phase peptide synthesis
manufacturer/tradename
Novabiochem®
mp
70-73 °C
application(s)
peptide synthesis
functional group
amine
storage temp.
2-8°C
SMILES string
Clc1c(cccc1)COC(=O)NCCCCC(NC(=O)OC(C)(C)C)C(=O)O
InChI
1S/C19H27ClN2O6/c1-19(2,3)28-18(26)22-15(16(23)24)10-6-7-11-21-17(25)27-12-13-8-4-5-9-14(13)20/h4-5,8-9,15H,6-7,10-12H2,1-3H3,(H,21,25)(H,22,26)(H,23,24)
InChI key
ATUMDPHEFWGCJF-UHFFFAOYSA-N
General description
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] K. Noda, et al. (1969) Bull. Chem. Soc. Jpn., 43, 1883.
[2] B. W. Erickson, et al. (1973) J. Am. Chem. Soc., 95, 3757.
Analysis Note
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in DMF): -12.0 - -10.0 °
Purity (TLC(011A)): ≥ 98 %
Purity (TLC(0811)): ≥ 98 %
Assay (HPLC, area%): ≥ 99.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Solubility (1mmoll in 2ml DCM): clearly soluble
Assay (acidimetric): ≥ 95.0 %
Enantiomeric purity: ≥ 99.5 % (a/a)
To see the solvent systems used for TLC of Novabiochem® products please click here.
Other Notes
Legal Information
Storage Class
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
Regulatory Information
This item has
Certificates of Analysis (COA)
Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.
Already Own This Product?
Find documentation for the products that you have recently purchased in the Document Library.
Protocols
Anhydrous HF is the preferred reagent for peptide cleavage from Boc-based resins, versatile and effective for various peptide synthesis.
Global Trade Item Number
| SKU | GTIN |
|---|---|
| 8530180100 | 04027269096366 |
| 8530180025 | 04027269096359 |