57017
Supelclean™ LC-SAX SPE Tube
bed wt. 500 mg, volume 3 mL, pkg of 54 ea
Synonym(s):
SAX tube
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About This Item
material
polypropylene tube
product line
Supelclean™
composition
bed wt., 500 mg
packaging
pkg of 54 ea
technique(s)
solid phase extraction (SPE): suitable
volume
3 mL
matrix
silica gel
matrix active group
SAX phase, quaternary amine, Cl- counterion
diameter
40-45 μm
pore size
60 Å
separation technique
ion exchange, ion exchange
Quality Level
application(s)
food and beverages
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Legal Information
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
Storage Class
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
dust mask type N95 (US), Eyeshields, Gloves
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Which document(s) contains shelf-life or expiration date information for a given product?
If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.
How do I get lot-specific information or a Certificate of Analysis?
The lot specific COA document can be found by entering the lot number above under the "Documents" section.
What is the functional group on the Supelclean LC-SAX SPE, Product 57017?
The Supelclean LC-SAX SPE functional group is an aliphatic quaternary amine bonded to silica, with a chloride (Cl-) counter-ion; the capacity is approximately 0.2 meq/g (milliequivalents per gram).
How can analytes be eluted from the Supelclean LC-SAX SPE, Product 57017?
The most common elution strategy with the Supelclean LC-SAX SPE is by pH manipulation. Start by using a buffer with the pH adjusted to at least 2 pH units above the molecule’s pKa. Methanol may be added to disrupt secondary interactions. Elute with 100 μL aliquots, at a reduced flow rate of approximately 1-2 drops/second.
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Articles
SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.
Protocols
Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.
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