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  • An efficient and cost-effective purification protocol for Staphylococcus aureus Cas9 nuclease.

An efficient and cost-effective purification protocol for Staphylococcus aureus Cas9 nuclease.

STAR protocols (2022-12-28)
Allen C T Teng, Marjan Tavassoli, Suja Shrestha, Ryan M Marks, Meghan J McFadden, Sonia L Evagelou, Kyle Lindsay, Ava Vandenbelt, Wenping Li, Evgueni Ivakine, Ronald Cohn, J Paul Santerre, Anthony O Gramolini
ABSTRACT

Here, we describe a protocol for purifying functional clustered regularly interspaced short palindromic repeats (CRISPR)-associated protein 9 (Cas9) from Staphylococcus aureus within 24 h and over 90% purity. SaCas9 purification begins with immobilized metal affinity chromatography, followed by cation exchange chromatography, and ended with centrifugal concentrators. The simplicity, cost-effectiveness, and reproducibility of such protocols will enable general labs to produce a sizable amount of Cas9 proteins, further accelerating CRISPR research.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
HEPES, ≥99.5% (titration)
Millipore
Benzonase® Nuclease, ≥250 units/μL, ≥90% (SDS-PAGE), recombinant, expressed in E. coli, buffered aqueous glycerol solution