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  • Synthesis of glycoluril catalyzed by potassium hydroxide under ultrasound irradiation.

Synthesis of glycoluril catalyzed by potassium hydroxide under ultrasound irradiation.

Ultrasonics sonochemistry (2009-05-27)
Ji-Tai Li, Xiao-Ru Liu, Ming-Xuan Sun
ABSTRACT

Synthesis of the glycolurils catalyzed by potassium hydroxide was carried out in 17-75% yield at 40 degrees C in EtOH under ultrasound irradiation. Compared to the method using stirring, the main advantage of the present procedure is milder conditions and shorter reaction time.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Glycoluril, 97%