- [Peculiarities of tetramethyltiuram disulfide detection in the biological material].
[Peculiarities of tetramethyltiuram disulfide detection in the biological material].
Sudebno-meditsinskaia ekspertiza (2010-06-22)
V K Shormanov, A V Kim, E P Duritsyn, Iu N Baranov
PMID20560513
ABSTRACT
Optimal conditions for the extraction of tetramethyltiuram disulfide (TMTD) from biological materials with ethylacetate are described. The isolated compound can be separated from co-extracted impurities on a silicagel L (40/100 mcm) column. Identification and quantitative determination of TMTD purified from cadaverous liver were performed using thin-layer chromatography, IR spectrophotometry, and high performance liquid chromatography with UF detection.