- Preparation of acetonides from soybean oil, methyl soyate, and fatty esters.
Preparation of acetonides from soybean oil, methyl soyate, and fatty esters.
Journal of agricultural and food chemistry (2011-03-08)
Atanu Biswas, Brajendra K Sharma, Karl Vermillion, J L Willett, H N Cheng
PMID21375297
ABSTRACT
This paper describes the preparation of a new type of branched vegetable oil and its methyl ester that involves the formation of acetonides. A facile and environmentally friendly synthesis has been found to produce acetonides that entails the use of ferric chloride as a catalyst and is conducted at room temperature. The products have been fully characterized with the help of model compounds, including elemental analysis, infrared (IR) spectroscopy, nuclear magnetic resonance (NMR), and gas chromatography-mass spectrometry (GC-MS).
MATERIALS
Product Number
Brand
Product Description
Supelco
trans-9,12-Octadecadienoic acid methyl ester, certified reference material, 10 mg/mL in heptane
Supelco
cis-9,cis-12-Octadecadienoic acid methyl ester, certified reference material, 10 mg/mL in heptane