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[Chemical constituents from Exochorda racemosa].

Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica (2011-08-17)
Jiajia Zhang, Xiangmei Li, Lihua Ren, Chengwu Fang, Fei Wang
ABSTRACT

To study the chemical constituents of Exochorda racemosa. Compounds were isolated and purified by silica gel, Sephadex LH-20, MCI gel and RP-18 column chromatography, and their structures were determined by spectroscopic analysis. Twenty compounds were isolated and identified as N-p-coumaroyl-N'-caffeoylputrescine (1), sutherlandin trans-p-coumarate (2), apigenin 7-O-methylglucuronide (3), astragalin (4), nicotiflorin (5), kaempferol 3-neohesperidoside (6), rutin (7), apigenin (8), luteolin (9), linalool-1-oic acid (10), betulalbuside A (11), ursolic acid (12) , corosolic acid (13), gynuramide II (14), beta-sitosterol (15), daucosterol (16), uridine (17), adenosine (18), syringin (19), and trans4-hydroxycinnamic acid (20), respectively. All compounds were obtained from this plant for the first time, moreover, 1 was reported as a new natural product, and 2 is a naturally rare cyanogenic glycoside.

MATERIALS
Product Number
Brand
Product Description

Supelco
β-Sitosterol β-D-glucoside, analytical standard
Sigma-Aldrich
Corosolic acid from Lagerstroemia speciosa, ≥98% (HPLC)
Supelco
Eleutheroside B, analytical standard
Sigma-Aldrich
Kaempferol 3-β-D-glucopyranoside, ≥97.0% (HPLC)