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  • [Analyze on chemical compositions of Dalbergia odorifera essential oils extracted by CO2-supercritical-fluid-extraction and steam distillation extraction].

[Analyze on chemical compositions of Dalbergia odorifera essential oils extracted by CO2-supercritical-fluid-extraction and steam distillation extraction].

Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials (2012-04-18)
Wei-Feng Song, Mei-Jin Liao, Shu-Yuan Luo
ABSTRACT

To analyze the chemical compositions of Dalbergia odorifera essential oils extacted by CO2-supercritical-fluid-extraction (SFE-CO2) and steam distillation extraction (SD). The essential oils of Dalbergia odorifera were extracted by steam distillation extraction and SFE-CO2. The chemical components were separated and analyzed by gas chromatography-mass spectrometry. 12 compounds were identified in SFE sample. The major components from essential oils were 2-propenoic acid-3(4-methoxyphenyl)-ethyl ester (14.53%), nerolidol (14.95%), ageratochromene (1.33%). 9 compounds were identified in SD sample. The major components from essential oils were nerolidol (26.61%), cedrol (1.65%). The SFE method is better than the SD method in reliability stability and reproducibility, and suitable for essential oils extraction of Dalbergia odorifera.

MATERIALS
Product Number
Brand
Product Description

Supelco
trans-Nerolidol, analytical standard
Sigma-Aldrich
Nerolidol, mixture of cis and trans, ≥97%, stabilized, FG
Sigma-Aldrich
Nerolidol, 98%, Mixture of cis and trans
Sigma-Aldrich
(+)-Cedrol, ≥99.0% (sum of enantiomers, GC)