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  • The effects of environment and cyclic fatigue on the mechanical properties of an indirect composite.

The effects of environment and cyclic fatigue on the mechanical properties of an indirect composite.

Journal of dentistry (2012-06-23)
Ryan K Hurley, James L Drummond, Grace C Viana, Maria T Galang
ABSTRACT

The purpose of this study was to examine the flexure strength (σ) and fracture toughness (K(IC)) of three indirect dental composites (dentin, body, and incisal) with respect to loading (static and cyclic), testing environments (air and water) and ageing (0 (controls) and 6 months in air and water). The specimens were 3 mm × 3 mm × 25 mm bars with the fracture toughness specimens having a 0.75 mm notch machined in the midspan. Static testing utilized 15 bars and cyclic testing 25 bars for each testing variable. All bars were tested using three-point loading and the cyclic testing was for 1000 cycles using a staircase approach. For flexure strength and fracture toughness, all specimen groups showed a decrease in mean values when exposed to cyclic loading as compared to the static loading mean and when exposed to ageing compared to the control specimens. ANOVA analysis demonstrated that dentin specimens had higher flexure strength and fracture toughness means than incisal and body specimens and that control and water specimens had higher flexure strength and fracture toughness means than aged and air specimens. Degradation of these materials, as a result of cyclic loading and ageing in an aqueous environment, appears to be influenced by more than just the processing of the composite.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Bisphenol A ethoxylate dimethacrylate, average Mn ~1,700, EO/phenol 15, contains 200 ppm MEHQ as inhibitor
Sigma-Aldrich
Triethylene glycol dimethacrylate, contains 80-120 ppm MEHQ as inhibitor, 95%
Sigma-Aldrich
Triethylene glycol dimethacrylate, contains 200 ppm monomethyl ether hydroquinone as inhibitor, 99%