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Merck
CN

[Study on the chemical constituents of Herpetospermum caudigerum].

Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials (2012-12-21)
Bing Xu, Pan-Pan Yang, Pei-Long Wang, Hu-Lang Ling, Min Chen
ABSTRACT

To study the chemical constituents of Herpetospermum caudigerum. The chemical constituents were isolated by silica gel, Sephedex LH-20 and MCI methods. Their structures were elucidated by physical-chemical properties and spectroscopic methods such as UV, IR, ESI-MS, H-NMR and 13 C-NMR. Seven compounds were isolated and identified as Herpetolide A (1), Herpetolide B (2), Dehydrodiconiferyl alcohol (3), Herpetol (4), Arbutin, 1-acetate (5), Dodecanoic acid (6) and 10-Eicosenoic acid (7). compounds 5-7 are isolated from this plant for the first time.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Lauric acid, natural, ≥98%, FCC, FG
Sigma-Aldrich
Lauric acid, ≥98%, FCC, FG
Sigma-Aldrich
Sodium dodecanoate, 99-100%
Supelco
Dodecanoic acid, analytical standard
Sigma-Aldrich
Dodecanoic acid, 98%
Sigma-Aldrich
Dodecanoic acid, ≥99% (GC/titration)