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  • Degree of conversion of polymer-matrix composite assessed by FTIR analysis.

Degree of conversion of polymer-matrix composite assessed by FTIR analysis.

The journal of contemporary dental practice (2013-04-13)
Mateus Rodrigues Tonetto, Shelon Cristina Souza Pinto, Alessandra de Nara Souza Rastelli, Alvaro Henrique Borges, José Roberto Cury Saad, Fábio Luis Miranda Pedro, Marcelo Ferrarezi de Andrade, Matheus Coelho Bandéca
ABSTRACT

The behavior of polymer-matrix composite is dependent on the degree of conversion. The aim of this study was to evaluate the degree of conversion of two resin cements following storage at 37°C immediately, 24 and 48 hours, and 7 days after light-curing by FTIR analysis. The specimens were made in a metallic mold and cured with blue LED with power density of 500 mW/ cm(2) for 30 seconds. The specimens were pulverized, pressed with KBr and analyzed with FTIR following storage times. ANOVA (two-way) and Tukey's post hoc. To the polymer-matrix composites between 24 and 48 hours does not show a significant increase (p > 0.05), however, the highest values were found after 7 days. The polymer-matrix composites used in this study showed similarity on the degree of conversion and increased of according to the time of storage.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
2-Hydroxyethyl methacrylate
Sigma-Aldrich
Triethylene glycol dimethacrylate, contains 80-120 ppm MEHQ as inhibitor, 95%
Sigma-Aldrich
2-Hydroxyethyl methacrylate, ≥99%, contains ≤50 ppm monomethyl ether hydroquinone as inhibitor
Sigma-Aldrich
2-Hydroxyethyl methacrylate, contains ≤250 ppm monomethyl ether hydroquinone as inhibitor, 97%
Sigma-Aldrich
Triethylene glycol dimethacrylate, contains 200 ppm monomethyl ether hydroquinone as inhibitor, 99%