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LaNiO3 nanotubes produced using a template-assisted method.

Journal of nanoscience and nanotechnology (2014-04-18)
A Zenatti, J F Queiruga Rey, A C Lanfredi, E R Leite, E Longo, M T Escote
ABSTRACT

We have studied the experimental conditions needed to produce LaNiO3 (LNO) nanostructures using a template-assisted method. In this route, a mesoporous anodic aluminum oxide template was filled with a chemical solution that had been prepared with polymeric precursors route. The precursor solutions and synthesized samples were characterized by X-ray diffraction (XRD), thermogravimetric analysis, infrared spectroscopy and high-resolution scanning electron microscopy (HRSEM). The XRD results for the samples that were heat-treated at 700 degrees C revealed that these samples crystallize in a perovskite-like LaNiO3 structure. HRSEM images revealed that the samples prepared with different deposition times (0.5, 1 and 2 h) promoted the formation of LaNiO3 nanotubes with different wall thicknesses.

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Sigma-Aldrich
Lithium niobate, 99.9% trace metals basis