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  • Determination of phthalate diesters and monoesters in human milk and infant formula by fat extraction, size-exclusion chromatography clean-up and gas chromatography-mass spectrometry detection.

Determination of phthalate diesters and monoesters in human milk and infant formula by fat extraction, size-exclusion chromatography clean-up and gas chromatography-mass spectrometry detection.

Journal of pharmaceutical and biomedical analysis (2017-09-26)
Massimo Del Bubba, Claudia Ancillotti, Leonardo Checchini, Donatella Fibbi, Daniele Rossini, Lorenzo Ciofi, Luca Rivoira, Claudio Profeti, Serena Orlandini, Sandra Furlanetto
ABSTRACT

A sensitive and reliable analytical method was developed for the simultaneous determination of five phthalate diesters and corresponding monoesters in human milk samples and infant formulas. The method involved a liquid-liquid extraction with a CH

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
1,3-Propylene sulfite, 99%
Supelco
mono-Benzyl phthalate, analytical standard