233234
2-氯-1-氟-4-硝基苯
98%
别名:
2-Chloro-1-fluoro-4-nitrobenzene
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关于此项目
线性分子式:
ClC6H3(F)NO2
化学文摘社编号:
分子量:
175.54
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
206-499-3
MDL number:
Assay:
98%
Form:
solid
InChI key
DPHCXXYPSYMICK-UHFFFAOYSA-N
InChI
1S/C6H3ClFNO2/c7-5-3-4(9(10)11)1-2-6(5)8/h1-3H
SMILES string
[O-][N+](=O)c1ccc(F)c(Cl)c1
assay
98%
form
solid
Quality Level
General description
2-Chloro-1-fluoro-4-nitrobenzene undergoes reduction in the presence of Mo(CO)6 and 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) under microwave irradiation to yield a mixture of 3-chloro-4-fluoroaniline and 3-chloro-4-ethoxyaniline.
Application
2-Chloro-1-fluoro-4-nitrobenzene has been used in synthesis of:
- benzoimidolones on Ameba resin
- methyl 6,7,8,9-tetrahydropyrido[1,2-a]indol-10-ylacetate
signalword
Danger
hcodes
Hazard Classifications
Acute Tox. 4 Oral - Eye Dam. 1 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
11 - Combustible Solids
wgk
WGK 3
flash_point_f
235.4 °F - closed cup
flash_point_c
113 °C - closed cup
ppe
dust mask type N95 (US), Eyeshields, Gloves
Practical and efficient synthesis of N-fused tricyclic indoles.
Koay N, et al.
Tetrahedron Letters, 52(1), 122-124 (2011)
Microwave mediated reduction of heterocycle and fluorine containing nitroaromatics with Mo (CO)6 and DBU.
Spencer J, et al.
Tetrahedron, 64(44), 10195-10200 (2008)
Microwave-assisted traceless synthesis of benzimidazolones.
Xu X-J and Zong Y-X.
Tetrahedron Letters, 48(1), 129-132 (2007)
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