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Merck
CN

C-144

Supelco

大麻二酚酸标准液 CRM 溶液

1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

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关于此项目

经验公式（希尔记法）:
C22H30O4
化学文摘社编号:
1244-58-2
分子量:
358.47
EC 号:
200-835-2
MDL编号:
MFCD09838337
UNSPSC代码:
41116107
NACRES:
NA.24

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等级

certified reference material

质量水平

300

表单

liquid

特点

(Snap-N-Spike®)

包装

ampule of 1 mL

制造商/商品名称

Cerilliant®

浓度

1.0 mg/mL in acetonitrile

技术

gas chromatography (GC): suitable
liquid chromatography (LC): suitable

应用

cannabis testing
cannabis testing

包装形式

single component solution

运输

dry ice

储存温度

−70°C

SMILES字符串

Oc1c(c(cc(c1C(=O)O)CCCCC)O)[C@H]2[C@@H](CCC(=C2)C)C(=C)C

InChI

1S/C22H30O4/c1-5-6-7-8-15-12-18(23)20(21(24)19(15)22(25)26)17-11-14(4)9-10-16(17)13(2)3/h11-12,16-17,23-24H,2,5-10H2,1,3-4H3,(H,25,26)/t16-,17+/m0/s1

InChI key

WVOLTBSCXRRQFR-DLBZAZTESA-N

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相关类别

一般描述

这种认证的峰值溶液® 适用于通过GC/MS，LC/MS或HPLC进行大麻二酚酸测定，从而用于大麻效力或杂质分析、药物研究和法医分析等应用。Cerilliant溶液，大麻素的认证参考物质（CRM），以方便、定量、US-DEA豁免的溶液形式提供，并为加拿大客户提供TK＃s。

大麻二酚酸(CBDA)是 大麻 家族（如大麻和大麻草）植物中发现的主要大麻素之一。它主要存在于植物的叶片中，在存在光和热的作用下脱羧形成大麻二酚（CBD）。已知它显示出抗焦虑、抗炎、抗痛觉过敏、止吐、神经保护和抗惊厥活性。

应用

溶液形式的认证标准物质（CRM）可用于以下实验：
  • 使用反相高效液相色谱（RP-HPLC）结合二极管阵列检测器（DAD）测定油基质中的四种大麻素
  • 使用HPLC结合UV检测器鉴定和评估大麻籽油样品中主要含有的七种大麻素
  • 使用液-液萃取和HPLC-DAD分离和测定大麻油样品中的CBD和CBDA
  • 根据人用药品技术要求国际协调理事会（ICH）分析方法验证的三方指南，通过HPLC-UV法对不同大麻品种的生物质和提取物中的11种大麻素进行多重分析
  • 开发和验证使用HPLC-DAD法同时分析印度大麻和印度大麻提取物样品中的五种主要中性和酸性大麻素
  • 使用气相色谱-质谱（GC-MS）分析大麻花序中十种主要大麻素经甲硅烷基化和酯化后的衍生物

特点和优势

  • 表征过程完全经ISO/IEC 17025和ISO 17034认证。
  • 附有一份全面的分析证书(CoA)，数据包含稳定性、均匀性、浓度准确度、不确定性和可追溯性
  • 通过实时稳定性研究进行严格测试，以确保准确性和保质期
  • 使用合格的精密天平进行重量分析，以确保最小的不确定性
  • 在氩气火焰下密封安瓿瓶，可长期保存
  • 以方便的且DEA豁免的形式提供，以提高实验室效率

法律信息

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany
CERTIFIED SPIKING SOLUTION is a registered trademark of Cerilliant Corporation
Snap-N-Spike is a registered trademark of Merck KGaA, Darmstadt, Germany

象形图

FlameExclamation mark
GHS02,GHS07

警示用语：

Danger

危险分类

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Eye Irrit. 2 - Flam. Liq. 2

储存分类代码

3 - Flammable liquids

WGK

WGK 2

闪点(°F)

35.6 °F - closed cup

闪点(°C)

2.0 °C - closed cup

法规信息

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A simple, fast, and green oil sample preparation method for determination of cannabidioloic acid and cannabidiol by HPLC-DAD
Madej K, et al.
Separations, 7, 60-60 (2020)
Quantitative determination of CBD and THC and their acid precursors in confiscated cannabis samples by HPLC-DAD}, author={Hadener, M, et al.
Hadener, M, et al.142-150
Forensic Science International, 299, 142-150 (2019)
HPLC-DAD analysis of hemp oil supplements for determination of four cannabinoids: Cannabidiol, cannabidiolic acid, cannabinol and delta 9-Tetrahydrocannabinol
Madej K, et al.
Separations, 8, 227-227 (2021)
Federica Pigliasco et al.
Molecules (Basel, Switzerland), 25(16) (2020-08-14)
The aim of this work is to evaluate volumetric absorptive microsampling (VAMS) from capillary blood as an alternative strategy for therapeutic drug monitoring (TDM) in patients treated with the newly available GW-purified form of cannabidiol (Epidiolex®). A fast ultra-high-performance liquid
Alice Palermiti et al.
Pharmaceuticals (Basel, Switzerland), 14(5) (2021-06-03)
Medical cannabis is increasingly being used in the treatment and support of several diseases and syndromes. The quantitative determination of active ingredients (delta-9 tetrahydrocannabinol, THC, and cannabidiol, CBD) in galenic oily preparations is prescribed by law for each produced batch.

商品

Cannabinoid CRMs: Testing Accuracy & Traceability

ISO-certified cannabinoid CRMs, THC and THCA, available as single components or mixes, for accurate potency testing.

UHPLC Analysis of Cannabinoids

Cannabis products need cannabinoid characterization. Ascentis Express C18 resolves 14 similar cannabinoids in under seven minutes with excellent peak shape.

Optimizing for High Throughput Analysis of Cannabinoids in a Variety of Matrices Using Ascentis® Express C18 Column

A complete workflow for the HPLC separation of 17 cannabinoids in different cannabis products using Ascentis® Express C18 Column in a shorter run time with retention time stability. Learn more here.

Cannabis Potency Testing: Method Dev. & Cost Considerations

Overview of gradient HPLC-based cannabinoid analysis optimized for key method parameters.

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实验方案

Analysis of Active Cannabis Compounds

HPLC-UV analysis of active compounds in marijuana-infused edibles for potency testing; complex matrix requires precise methods.

Analysis of 17 Cannabinoids in Hemp and Cannabis

HPLC separation of 17 important cannabinoids including CBD, delta 9 THC and THCA. Read the application note.

UHPLC Analysis Cannabinoids Ascentis Express

Cannabis products need cannabinoid characterization. Ascentis Express C18 resolves 14 similar cannabinoids in under seven minutes with excellent peak shape.

Analysis of Active Cannabis Compounds (Cannabinoids) in Edible Food Products: Gummy Bears and Brownies

Rapid potency testing of marijuana-infused edibles using LC/MS on a biphenyl stationary phase detected eleven cannabinoids.

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