20639
Di-tert-butyl 1-(tert-butylthio)-1,2-hydrazinedicarboxylate
≥99.0% (HPLC)
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About This Item
Empirical Formula (Hill Notation):
C14H28N2O4S
CAS Number:
Molecular Weight:
320.45
NACRES:
NA.22
PubChem Substance ID:
eCl@ss:
32110502
UNSPSC Code:
12352108
MDL number:
Beilstein/REAXYS Number:
9559826
InChI
1S/C14H28N2O4S/c1-12(2,3)19-10(17)15-16(21-14(7,8)9)11(18)20-13(4,5)6/h1-9H3,(H,15,17)
SMILES string
CC(C)(C)OC(=O)NN(SC(C)(C)C)C(=O)OC(C)(C)C
InChI key
MOWYOPQOADUFLA-UHFFFAOYSA-N
assay
≥99.0% (HPLC)
mp
98-100 °C
application(s)
peptide synthesis
Other Notes
Stable reagent for the preparation of asymmetric S-tert-butyl disulfide derivatives (e.g. for the introduction of S-tert-butylthio protection into cysteine peptides) in organic solvents
Storage Class
13 - Non Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves, type N95 (US)
Regulatory Information
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E Wünsch et al.
Hoppe-Seyler's Zeitschrift fur physiologische Chemie, 363(12), 1461-1464 (1982-12-01)
The sterically hindered tert-butyl thiol reacts smoothly with azodicarboxylic acid derivatives only upon addition of catalytic amounts of sodium alcoholate, yielding crystalline and analytically well characterized 1-(tert-butylthio)-1,2-hydrazinedicarboxylic acid derivatives. These sulfur-activated reagents were found to be stable on storage and
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