238139
1-Iodonaphthalene
97%
Synonym(s):
1-Naphthyl iodide
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About This Item
Empirical Formula (Hill Notation):
C10H7I
CAS Number:
Molecular Weight:
254.07
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
201-968-9
Beilstein/REAXYS Number:
1906415
MDL number:
Product Name
1-Iodonaphthalene, 97%
InChI key
NHPPIJMARIVBGU-UHFFFAOYSA-N
InChI
1S/C10H7I/c11-10-7-3-5-8-4-1-2-6-9(8)10/h1-7H
SMILES string
Ic1cccc2ccccc12
assay
97%
refractive index
n20/D 1.701 (lit.)
bp
163-165 °C/15 mmHg (lit.)
density
1.74 g/mL at 25 °C (lit.)
functional group
iodo
Quality Level
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General description
Ultrafast relaxation of 1-iodonaphthalene has been studied by time-resolved femtosecond pump-probe mass spectrometry. 1-Iodonaphthalene undergoes Pd catalyzed cross-coupling reaction (Stille reaction) with 2,4-dimethoxy-6-(trimethylstannyl)pyrimidine to afford 2,4-dimethoxy-6-(naphthalen-1-yl)pyrimidine.
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2
Storage Class
10 - Combustible liquids
wgk
WGK 3
flash_point_f
235.4 °F - closed cup
flash_point_c
113 °C - closed cup
ppe
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
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Javier I Bardagí et al.
The Journal of organic chemistry, 73(12), 4491-4495 (2008-05-21)
From the commercial 6-chloro-2,4-dimethoxypyrimidine (1) and by a photostimulated reaction with Me(3)Sn(-) ions, 2,4-dimethoxy-6-(trimethylstannyl)pyrimidine (2) was obtained in 95% yield. By the cross-coupling reaction of 2 with 1-iodonaphthalene as electrophile catalyzed by Pd (Stille reaction), 2,4-dimethoxy-6-(naphthalen-1-yl)pyrimidine (9) was obtained in
Raul Montero et al.
Physical chemistry chemical physics : PCCP, 12(28), 7988-7993 (2010-06-03)
The ultrafast relaxation of 1-iodonaphthalene, with particular attention to the dissociation channels, has been studied by time-resolved femtosecond pump-probe mass spectrometry following excitation at 267 and 317 nm. The measured transients for the parent ion and the isobaric fragments, iodine
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