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Sigma-Aldrich

Iodocyclohexane

98%

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Synonym(s):
Cyclohexyl iodide
Empirical Formula (Hill Notation):
C6H11I
CAS Number:
626-62-0
Molecular Weight:
210.06
Beilstein:
1900797
EC Number:
210-957-8
MDL number:
MFCD00003826
PubChem Substance ID:
24854149
NACRES:
NA.22

Quality Level

100

Assay

98%

form

liquid

contains

copper as stabilizer

refractive index

n20/D 1.5441 (lit.)

bp

80-81 °C/20 mmHg (lit.)

density

1.624 g/mL at 25 °C (lit.)

storage temp.

2-8°C

SMILES string

IC1CCCCC1

InChI

1S/C6H11I/c7-6-4-2-1-3-5-6/h6H,1-5H2

InChI key

FUCOMWZKWIEKRK-UHFFFAOYSA-N

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General description

The photodissociation dynamics of iodocyclohexane has been studied using velocity map imaging. Nickel catalyzed coupling of iodocyclohexane with 1-octyne has been investigated.

Application

Iodocyclohexane has been employed as reagent in demethylation of aryl methyl ethers in DMF under reflux condition.

Storage Class Code

10 - Combustible liquids

WGK

WGK 3

Flash Point(F)

158.0 °F - closed cup

Flash Point(C)

70 °C - closed cup

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

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Jun Yi et al.
Angewandte Chemie (International ed. in English), 52(47), 12409-12413 (2013-10-12)
A nicked reaction: The title reaction of terminal alkynes with non-activated secondary alkyl iodides and bromides was accomplished for the first time. This reaction provides a new and practical approach for the synthesis of substituted alkynes (see scheme; cod=cyclo-1,5-octadiene).
An efficient method for demethylation of aryl methyl ethers.
Zuo L, et al.
Tetrahedron Letters, 49(25), 4054-4056 (2008)
D K Zaouris et al.
The Journal of chemical physics, 135(9), 094312-094312 (2011-09-15)
The photodissociation dynamics of iodocyclohexane has been studied using velocity map imaging following excitation at many wavelengths within its A-band (230 ≤ λ ≤ 305 nm). This molecule exists in two conformations (axial and equatorial), and one aim of the

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